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MCYIMUM VERMCATlON LABORATORY ANALYSIS 6 E- S; <br /> TANNK TANK TPH-G TPH-D BTX& E CL HC TOTAL EDB METALS PCB <br /> CONTEN#"S 8015 8015 $020 8010 LEAD ICA21 8270 <br /> 8260 8260 8260 8240 7424 8240 AFS or 8080 <br /> 7421 AA <br /> LEADED <br /> GAS X X X X <br />.61 LJN-L GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UN-K FUEL X X X X X <br /> PROD OIL X X <br /> CHLOR <br /> SOLVENTS X X <br /> lr O lv CHLO R <br /> SOLVENTS X X X <br /> w.asTE� <br /> l USED OIL X XX X X X <br /> All analyses methods are designated EPA methods described in EPA SW 846, Thud Ediuon 'Those methods not found <br /> in SW 346, are speaficaily noted below Refer to the "SV/RCB LUFT Field Manual", Appendix A-20, Table 3-5 for <br /> detection limits of rotor vehicle fuels (gasoline and diesel) Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil detection Limits <br /> etection Limits that remain below the 1ffCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method <br /> LA.BOFATORYANALYSES TERNfLNOLOGY <br /> X TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8315 mod or GC1,MS 8260 <br /> X TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FM (3550), 8015 mod or GGMS 8260 <br /> �{ BTX & E Benzene, Toluene, Xylene & Ethyl Benzene, GCIPID 80'20 or GC1MS 8260 <br /> X CL HC Chlonnated Hydrocaxbon, GCIHSD 8010, GCIMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene diororrude (DHS-AB ISM), GCIMS 8240 (DHS-LLFM <br /> GC-FID Gas Chromatography, Flame Ionization Detecuon <br /> 7( ICRP or AA Inductively Coupled Plasma Atomic Emission Spernrometry 6010 or Atomic Absorption <br /> Spectrometry 7000 Metals: Cadmium, Chromium III and VL Lead, Zinc and Nickel. <br /> X PCS Polychlonnated Biphenyls, GCIMS 8270 or SM <br /> Method 3050 Acrd digesaotx <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> Q-VQC Quality Assurance/Quality Control <br /> Notes To avoid false positive detection of benzene, benzene-free solvents are to be used- Fused capillary columns are <br /> preterred to packed columns, a packed column may be used as a 'first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> ries because the detection limits are lower and the QAIQC is better Samples exhibiting any level of heavy metal <br /> ootamination may require further analysis. PISS-EHD recommends holding these samples until disposal is indicated- <br /> EH 23 043 (Revised 7/10192) Page 8 <br />