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Alpha Analytical Laboratories Inc. 860 Waugh Lane, H-1, Ukiah, California 95482 <br /> (707) 468-0401 <br /> CHEMICAL EXAMINATION REPORT <br /> San Joaquin Co. Public Health' Serv. <br /> Environmental Health Division <br /> P.O. Box 388 Date Printed Page <br /> Stockton, CA 95201-0388 11/04/96 5 <br /> Attn: Letitia Briggs <br /> Batch Number Receipt Date Client Client P.O. Send Via <br /> 96-1022-009 10/21/96 17:10 ADVGEO Mail <br /> METHOD EXTRACTED TEST DATE RESULT UNITS PQL DILUTION <br /> (continued from previous page) <br /> Sample 3 #3,4,5 Tank 3 S.P. Composite <br /> National Freight, Inc. <br /> Sample Type: Soil Sampled by: Phillips/Cuellar Sampled: 10/21/96 15:40 <br /> Analysis of this sample .also indicates the presence of <br /> hydrocarbons higher in molecular weight than diesel. <br /> * Additional notes for this Sample are printed at the conclusion of the Results Report. <br /> TPH Gasoline W/BTXE <br /> TPH - Gasoline GCFIO/5030 10/24 10/24/96 ND ug/g 1.00 <br /> Benzene EPA 8020 10/28 10/28/96 ND ug/g .005 <br /> Toluene EPA 8020 10/28 10/28/96 ND ug/g .005 <br /> Ethylbenzene EPA 8020 10/28 10/28/96 ND ug/g .005 <br /> Xylenes EPA 8020 10/28 10/28/96 NO ug/g .005 <br /> TPH - Diesel 8015/MOD 10/31 10/31/96 2.4 ug/g 1 <br /> Metals <br /> Lead EPA 6010 11/01/96 7.8 mg/kg 5.0 <br /> Chromium EPA 6010 11/01/96 20 mg/kg 5.0 <br /> Cadmium EPA 6010 11/01/96 ND mg/kg 1.0 <br /> Nickel EPA 6010 11/01/96 17 _ mg/kg 10.0 <br /> Zinc EPA 6010 11/01/96 42 mg/kg 10.0 <br /> PCB s EPA8080 10/24 10/24/96 NO ug/g .2 <br /> Halogenated Volatile Organics EPA8010 10/24/96 <br /> Bromodichloromethane . . . . . . ND ug/g .005 <br /> Bromoform <br /> ND u9/9 .005 <br /> PQL Practical Quantitation Limit ND - None Detected <br /> * - indicates Detection Limit altered due to Sample Dilution <br /> I <br /> NOTES: <br /> *** SECOND COPY *** <br /> Bruce L. Gove <br /> Laboratory Director Date Printed: 11/04/96 <br /> i <br />