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CERTIFICATE OF ANALYSIS <br /> /4178ry�'%Cel/ Laboratory - <br /> Tuesday,]4TurcG 12, 2002 <br /> TO: William Little <br /> Advanced GeoEnviron mental <br /> 837 Shaw Road <br /> Stockton CA 95215 <br /> Total Petroleum in Gasoline <br /> Sample.Information <br /> Sample ID: 14494-04C Sample Type: Grab <br /> Sample Description: Tank#2 South End Project Name: 4040 E.Main ST. <br /> Date/Time Sampled: 3/6/2002 3:25:00 PM Sample Matrix: Soil <br /> ANALYTICAL RESULT QAIQC.REPORT <br /> Date LCS Spike MS Spike <br /> Method DLR Unit Result Analyzed Blank Cone. LCS% Conc. MS% MSD RSD <br /> est Parameter <br /> TPH-Diesel EPA 8015MILDFT . .: ..,.500 , ug _...w,. <br /> /kg NQ 08-Mar-02 ND 5000 96.0% 5000 102.0% 104.0% 0$% <br /> ~ rngrl —milligrrrnas per Liter=ppm /dSD-rep resenl relative percew different(RPD)betxve'en duplicates spike vfsanaples <br /> ug%L=naicrngrrinrs per Liier=Ppb or Duplicate of S7ample <br /> REP CT. ULL MI ED, <br /> C Composite G Grab <br /> !VSIAISD-menswre of the percent recovery eff+cieneies s+iihin the matrix <br /> = = <br /> 1_CS-Measure of fire Percent recovea)'of fhe Laborurort Coaaarol spike(L(S') <br /> DLR-Deiecllon Limit for the Purpose of Reporting. Exceplivnat sample <br /> .1011 tl1 n Han V.Le,Laboratory Director naatrkes or iamerferene°ces mnv result in higher detection limits <br /> EPA-Fnvaronmc'nurl Prvlc:rtivm;} encs h9ethod. SA1-Strrnrtnrd Adcthod 1nr C.rarnrnativn of 11'nter }f uslcnxucr kSrh.ErL Page 1 &J, <br /> 545 E. Cleveland St. Suite A Stockton, CA 95204 Tel.: (209) 462-0892 Fax: (249) 462-7935 <br />