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Entcch Analytical Lads Inc. <br /> ' 3334 Victor Court , Santa Clara, CA 95054 Phone (408) 588-0200 Fax- (408) 588-0201 <br /> Quality Control - Method Blank <br /> QC Batch ID WMS5040728 <br /> Validated by MTU-07128104 Matrix Liquid <br /> Date of Analysts 7/28/2004 <br /> ' Method GC-MS <br /> Parameter Result DI, PQL PQI R Units <br /> TPH as Gasoline ND 1 25 25 lig/L <br /> ' Surrogate for Blank %Recovery Control f imW <br /> 4-Bromotluorobenzcnc 918 64 - 125 <br /> Dibromolluoromcthanc 983 23 - 172 <br /> 1 oluene-d8 993 70 - 134 <br /> ' Quality Control - Laboratory Control Spike 1 Duplicate Results <br /> ' Reviewed by M flJ-07128!04 QC Batch ID WMS5040728 <br /> Date of Analysts 7/28/2004 <br /> ' Method CC-MS Liquid Cone Units µg/L <br /> Parameter Blank Spike Amt SpikeResult QC Type Analysis Date %Recovery HPD RPD Limits Recovery Limeh <br /> fill!as Gasoline v_ — <25 — 1250 — 133 G — LCS 7/2812004 _1069 _ _ _65 135 — <br /> Surrogate %Recovery Control Limits <br /> 4-Bromufluorobcnwie %1 64 - 125 <br /> Dihromolluaromethane 907 23 - 172 <br /> —�Tnlucnf;-d8— — —99 1 70 50 134 <br /> TPH as Gasoline _ <25 1250 136 1 CSD 7128/2004 1088 l 8 25 GS 135 <br /> Surrogate %Recovery Control Limit, <br /> 4-BromofluorobenzLne 925 64 - 125 <br /> Dibromofluoromethane 907 23 - 172 <br /> Toluene d8 — — 998 — 70 134 <br /> 1 <br /> 1 <br /> 1 <br />