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AIf Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425 Lancaster,PA 17605-2425•717-656 2300 Fax 717 656.2681•WWW lancaSterlabS com <br /> Page ] of 2 <br /> Lancaster Laboratories Sample No. WW 4165115 <br /> MW-4-W-031111 Grab Water <br /> Facility# 91452 Job# 386582 GRD <br /> 334 E Main St Ripon 70607700554 MW-4 <br /> Collected 11/11/2003 09 19 by AS Account Number 10906 <br /> Submitted 11/14/2003 09 35 ChevronTexaco <br /> Reported 11/26/2003 at 15 44 6001 Bollinger Canyon Rd L4310 <br /> Discard 12/27/2003 San Ramon CA 94583 <br /> 334M4 <br /> As Received <br /> CAT. As Received Method Dilution <br /> No Analysis Name CAS Number Result Detection Units Factor <br /> Limit <br /> 01728 TPH-GRO - Waters n a 350 50 ug/l 1 <br /> The reported concentration of TPH-GRO does not include MTBE or other <br /> gasoline constituents eluting prior to the C6 (n-hexane) TPH-GRO range <br /> start time <br /> A site-specific MSD sample was not submitted for the project A LCS/hCSD <br /> was performed to demonstrate precision and accuracy at a batch level <br /> 01412 Methanol and Ethanol <br /> 01414 Methanol (by Direct Injection) 67-56-1 N D 1,000 ug/l 1 <br /> 01594 BTEX+5 Oxygenates+EDC+EDB+ETON <br /> 01587 Ethanol (54-17-5 N D 500 ug/l 5 <br /> 02010 Methyl Tertiary Butyl Ether 1634-04-4 3,700 25 ug/1 50 <br /> 02011 di-Isopropyl ether 108-20-3 N D # 3 ug/l 5 <br /> 02013 Ethyl t-butyl ether 637-92-3 N D # 3 ug/l 5 <br /> 02014 t-Amyl methyl ether 994-05-8 220 3 ug/l 5 <br /> 02015 t-Butyl alcohol 75-65-0 120 100 ug/l 5 <br /> 05401 Benzene 71-43-2 N D # 3 ug/1 5 <br /> 05402 1,2-Dichloroethane 107-06-2 N D # 3 ug/l 5 <br /> 05407 Toluene 108-88-3 N D # 3 ug/l 5 <br /> 05412 1,2-Dibromoethane 106-93-4 N D # 3 ug/l 5 <br /> 05415 Ethylbenzene 100-41-4 N D # 3 ug/l 5 <br /> 06310 Xylene {Total) 1330-20-7 N D # 3 ug/l 5 <br /> Due to the level of methyl t-butyl ether, the reporting limit(s) for <br /> all GC/MS volatile compounds were raised <br /> State of California Lab Certification No 2116 <br /> j Laboratory Chronicle <br /> CAT Analysis Dilution <br /> No Analysis Name Method Trial# Date and Time Analyst Factor <br /> 01728 TPH-GRO - Waters N CA LUFT Gasoline 1 11/17/2003 17 55 Martha L Seidel 1 <br /> Method <br /> 01412 Methanol and Ethanol SW-846 80153 1 11/19/2003 12 22 Tiffany A George 1 <br /> 01594 BTEX+5 SW-846 8260B 1 11/18/2003 11 26 Lauren C Marzario 5 <br /> Oxygenates+EDC+EDB+ETON <br /> 01594 BTEX+5 _ SW-846 82608 1 11/18/2003 11 53 Lauren C Marzario 500 <br /> ---- Oxygenates+EDC+EDB+ETOH = <br /> #=Laboratory MethodDetection Limit exceeded target detection limit <br /> N D=Not detected at or above the Reporting Limit <br />