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Analytical Laboratory CERTIFICATE OF ANALYSIS <br /> friday,July 02, 1999 <br /> Advanced Geo Environmental <br /> 4005 N. Wilson Way <br /> Stockton, CA. 95205 <br /> Sample Information <br /> Sample ID: PE5380-01 Sample Tjpe: Grab <br /> Sample Description: B 1@ 15' Project Name: ACME SAW&INDUSTRIAL <br /> Date/Thne Sampled.- 6/15/99 8:15:00 AM Sample Matrix: Soil <br /> ANALYTICAL RESULT ,., ;,,...:x,.. -,., .......:............ <br /> QA/ REPORT <br /> 'Test Date LCS Spike MS Spike <br /> Parameter <br /> Method <br /> DLR <br /> Unit <br /> i <br /> Result Drlutrorr Analyzed Blank Co 1c. LCS% Conc. MS% MSD RSD <br /> TPH-Gasoline EPA 8015M/DHS 1 mg/Kg17-Jun-99 <br /> ,..:.... ....... ... <br /> 17 Jun 99 ND 2 97.5% 2 90.0% 87.5% .•0.7% <br /> TPH Diesel EPA 8015M/DHS 1 m /K ND 1 • <br /> _::�.,:,.,---,,..,..,, 50 94.0% 50 .0% <br /> 8020 5 ND ......... <br /> Benzene EPA 6'/0 ... <br /> 17-Jun-99 ND <br /> u9/K9 1 17 Jun 99 ND5 84.0° 5 80.0% 82.0% 0.6% <br /> Toluene ,•:.::•:.:.,:::..,.::::::.,,,.::::::.:.:::.,•.,•:.,,:,,..:.::.:.:.,-w:.:.w.K:,..::•:N::.,.M» :.:..K..:.,.:.:.:::.,::.:..::.,:•.,-:::.::.::::::::::::.:::::.,•:. <br /> • EPA 8020 5 ug/Kg ND 1 17-Jun-99 ND 5 <br /> 98.0°!0 5 96.0% 102.0°k 1.0% : <br /> EEthylbenzene EPA 8020 :..........:,,•:.::.,,,•:::::::::.,,•.,:.:::::.:::.:•:.,•:::.:.v:.:,.:::•:,-.:.:.,-::.::.:.::•.:,..,..,•:::..:•::...,: -..: <br /> 5 ugJKg ND 1 17-Jun-99 ND 50...,: <br /> 102.0% 5 80.0% 92.0% 3.5/0 <br /> Xylenes Total <br /> EPA 8020 5 ug/Kg ND 1 <br /> 17-Jun-99 ND 10 92.0°✓a 10 91.0° 90.0°,6 0.3°6 <br /> Methyl-t-Butyl Ether(MtBE) EPA 8020 5 u /K ND 92...:.,>.>: ,::,:�,,.. :> ;,,,,.::...::.::,, ,•::::,:.:::..:.:.::•::.::.»:::::.`; <br /> .... <br /> ug/Kg 1 17-Jun-99 ND 5 92.0% 5 84.0°,6 86.0°,6 0.6°r6 <br /> mg1L=milligrams per Liter=ppm DLR-Detection Linrit forthe Purpose of RSD-represent relative ercent different h V <br /> 'tet P P (RPD)bet"wen duplicates spike of samples <br /> i, eg/L=micrograms per Liter=ppb. Reporting. Exceptional sample uudrices or or Duplicate of Sample <br /> C=Composite G=Grab interferences may result in higher detection AfRIMED-measure of the percent recovery efficiencies within the matrix <br /> lnnits <br /> LCS-measure ofthe percent recovery ofthe Laboratory Control Spike(LCS) <br /> RESPE TFULLY UB ITTED, <br /> Jonathan Hao V. Le,Laboratory Director <br /> ronruentalProtectionAgencpiLrcthorl. ,::•-^_a-,�M�.-A.•w.:.:, w..,•.,:-....._:..,:..:.,,.. ,... <br /> Page 1 of I <br /> �, ;, snr-St andar,ate,hadforLxmninatfot�Yt��'fijcEWWI j ^� �`+*�C •i.+-��wStockton, CA 95204 Tel.: (209) 462-0892 Fax: (209) 462-7935 <br />