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QC Report: Method Blank Data Report Number: 34728 Project Name : Former Beacon 12474 Date : 9/6/2003 Project Number: 1474.94 Method Parameter Measured Reporting Analysis Date Method Value t Units Method Analyzed Measured Reporting Analysis Date Benzene Parameter Value Limd Units Method Ana! zed Toluene <0.0050 0.0050 mg/Kg EPA 8260B 813012003 4 Bromofluarobenzene(Surr} 114<0.0050 0.0050 mg/Kg % EPA 82608 613112003 Ethylbenzene 91 9 EPA 82608 8!3012003 <0.0050 0.0050 mg/Kg EPA 82608 8!3012003 Total Xylenes Benzene <0.0050 0.0050 mg/Kg EPA 82608 8/30/2003 Toluene <0'50 0,50 uglL EPA 82608 813112003 Methyl-t-butyl ether(MTBE) <0,0050 0.0050 m K <0.50 0.50 ug/L EPA 82606 813112003 Diisopropyl ether(DIPS) < 9 EPA 82608 $13012003 Ethylbenzene <0.50 0.0050 0.0050 mg/Kg EPA 8260$ $13012003 Total Xylenes < 0.50 ug/L EPA 82608 8/31/2006 Ethyl-1-butyl ether(ETRE) <0.0050 0.0050 --mg1Kg EPA 8260B 813012003 0.50 0.50 ug1L EPA 8260$ 8!311200 Ethyl-l-bTert-arnymethyl ether(TAME) <0.0050 0.0050 mg1Kg EPA 82608 8/30/2003 Methyl-t-butyl ether(MTBE) <0.50 0.50 ug/L EPA 82608 8/31/2003 Tert-Butanol <0.0050 0.0050 mg/K9 EPA 826DB 8!30!2403 Diisopropyl ether(DIPE) <0.50 0.50 ug/L EPA 82608 813112003 Methanol <0.20 0.20 mg/Kg EPA 82608 8!30!2003 WNW ether(ETRE) <0.50 0,50 ug/L EPA 82608 8/31/2003 Ethanol Ter[-amyl methyl ether(TAME) <0.50 0,50 uglL EPA$2608 $13112003 <0.01a 0.010 mg/Kg EPA 82608 8/30/2003 Ter[-Butanol TPN as Gasoline <1.0 1.0 m91Kg EPA 8260B 813012003 Methanol <5.0 5.0 ug/L EPA 8260B 8/31/2003 1,2-Dichloroethane <0.0050 4.0050 m91 K Ethanol <50 50 ug/L EPA 82608 813112003 g EPA 82606 8/30/2003 1,2-Dibromoethane <0.0050 0.0050 mg/Kg EPA 82608 8/3012003 1,2-Dir <5.0 5.0 ug/L EPA 82608 8131/2003 Toluene-d8(Surr) <0.50 0.50 ug1L EPA 82608 8/31/2003 98.0 % EPA 82606 8!3012003 1,2-Dibromoethane <0.50 0.50 ug/L EPA 82606 8/31/2003 4-Bromofluorobenzene(Surr) 105 % EPA 82608 8/30/2003 TPH as Gasoline Dibromm olluoroethane(Sun) 98,5 ° <50 5o ug1L EPA 8260B 8/31/2003 � EPA 82608 8!30/2003 Toluene-d8(Surr) 1,2-DirWoroethane-d4(Surr) 100 103 EPA 82608 $13012003 4-8mmofluorobenzene(Surr) 105 � EPA 8260B 8/31/2003 % EPA 8260B 8/3112003 Benzene <0,50 0.50 uglL EPA 82608 8/31/2003 Benzene Toluene <0.50 0.50 ug/L EPA 8260$ 6/3112003 Toluene <0.50 0.50 ug1L EPA 82608 8/31!2003 Ethylbenzene <0.50 0.50 ug/L EPA 82606 el3t12a03 Ethylbenzene <0,50 0.50 uglL EPA 8260B 8/31/2003 Total Xylenes <0.50 0.50 u !L <0.50 0,50 ug/L EPA 82608 8/3112003 9 EPA 82608 8/3112003 Total Xylenes < Methyl-t-butyl ether(MTBE) <0.50 0.50 ug1L EPA 82608 8!3112003 Methyl-t-butyl ether(MTBE) <0.60 0.50 ugrL EPR 82608 8/3i/2003 Diisopropyl ether(DIPE) <0.50 0.50 ug/L EPA 82608 8/31/2003 Diisopropyl ether(DIPE) <0.50 0.50 ug/L EPA 826DB 8/31/2003 Ethyl-t-butyl ether(ETRE) <0.50 0.50 u !L 0.50 0.50 uglL EPA 82648 8131!2003 Tert-amyl methyl ether(TAME) < 9 EPA 82608 8/31/2003 Ethyl-1-butyl ether(ETRE) <0.50 0.50 0.50 0.50 ug1L EPA 826DB 8/31/2003 Tert-am I methyl ether TAME < ug/L EPA 8260B 8/31/2003 Tert-8utanof Y Y (TAME) 0.50 0.50 ug1L EPA 82608 8131!2003 <5.0 5.0 uglL EPA 82608 8/31/2003 Tert-Butanol Methanol <5050 uglL <5.0 5.0 ug/L EPA 82608 8131/2003 Ethanol EPA 82608 8131!2003 Methanol <50 <5'0 5.0 ug/L EPA 82608 8/31/2003 Ethanol 50 ug/L EPA 82606 8131/2003 1,2-Dichloroethane <0.50 0.50 uglL EPA 8260B 8131!2003 ,2•Dichloroelhane <5.0 5.0 ug/L EPA 8260E $/31120D3 1 1,2-Dibromoethane <0.50 0.50 u 1L <0.50 0.50 ug/L EPA 8260E 8131/2003 9 EPA 82606 8/31/2003 1,2-Dibromoethane TPN as Gasoline <0.50 0.50 ug/L EPA 82608 813112003 <50 50 ug/L EPA 8260B 8/31/2003 TPH a5 Gasoline Toluene-d8(Surr) <50 50 u9/L EPA 82606 8131/2003 11 94.9 % EPA 82608 8/31/2003 Toluene-d8(Surr) 105 % EPA 82608 813112003 a`� f KIFF ANALYTICAL, LLC Approved By: J 2795 2nd St. Suite 300 Davis- CA 95616 530.297-4800 �%