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r F Report Number 42780 QC Report Matrix Spike/Matrix Sprite Duplicate Date 3/18/2005 Protect Name Former Beacon 12474 Protect Number 1474.48 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent ap Sample eea Sample Sample Analysis Date vtvtcent Lt v Parameter Sample Vle LSpike veLLevl VuValUnits MethodAnalyzed RecoRecoplfimiLimit Benzene 42770-03 <0 50 400 400 445 439 ug/L EPA 8260B 3115105 111 110 1 31 70-130 25 Toluene 42770-03 <0 50 400 400 424 422 ug/L EPA 8260B 3115105 106 105 0 554 70-130 25 Tert-Butanol 42770-03 <5 0 200 200 210 213 ug/L EPA 8260E 3115105 105 106 146 70-130 25 Methyl-t-Butyl Ether 42770-03 1 1 400 400 402 41 6 ug/L EPA 8260B 3/15105 977 101 362 70-130 25 Benzene 42770-22 <0 50 400 400 446 427 ug/L EPA 82606 3/16/05 111 107 420 70-130 25 Toluene 42770-22 <0 50 400 400 42 0 404 ug/L EPA 8260B 3116105 105 101 371 70-130 25 Tert-Butanol 42770-22 <5 0 200 200 201 209 ug1L EPA 8260E 3116105 100 105 409 70-130 25 Methyl-t-Butyl Ether 42770-22 <0 50 400 400 42 3 41 1 ug/L EPA 8260B 3/16105 106 103 274 70-130 25 Benzene 42777-01 <0 50 400 400 382 376 ug/L EPA 8260B 3/14105 956 941 149 70-130 25 Toluene 42777-01 <0 50 400 400 361 357 ug/L EPA 8260B 3114/05 903 892 1 22 70-130 25 Tert-Butanol 42777-01 <50 200 200 194 192 uglL EPA 8260B 3114/05 970 960 1 07 70-130 25 Methyl-t-Butyl Ether 42777-01 <0 50 400 400 387 386 ug/L EPA 8260E 3114105 96 9 964 0 475 70-130 25 Benzene 42772.04 <0 50 400 400 389 38 8 ug/L EPA 8260B 3115105 972 971 0 165 70-130 25 Toluene 42772-04 <0 50 400 400 370 36 4 ug/L EPA 8260B 3/15/05 925 91 1 1 53 70-130 25 Tert-Butanol 42772-04 <5 0 200 200 191 191 ug/L EPA 8260E 3115/05 954 954 00827 70-130 25 Methyl-t-Butyl Ether42772-04 <0 50 400 400 39 7 394 ug/L EPA 8260B 3115/05 993 986 0 689 70-130 25 i KIFF ANALYTICAL, LLC Approved By Joe iff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800