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• • Paco Analytical Services,Inc. <br /> 9 2795 Sewnd Street-Suite 300 <br /> _ 2ceAnalAcal Davis,CA 95618 <br /> rmm•.pacelabs wra (530)297-4800 <br /> QUALITY CONTROL DATA <br /> Project: DIESEL LINE SAMPLING <br /> Pace Project No.: 1246740 <br /> QC Batch: DAVM/l303 Analysis Method: EPA 82608 <br /> QC Batch Method: EPA 5035/50306 Analysis Description: 8260 MSV Med UST <br /> Associated Lab Samples: 1246740001 <br /> METHOD BLANK: 208497 Matrix: Solid <br /> Associated Lab Samples: 1246740001 <br /> Blank Reporting <br /> Parameter Units Result Limit Analyzed Qualifiers <br /> Benzene mg/kg ND 0.25 05113/1514:31 <br /> Diisopropyl ether mg/kg ND 0.25 05/1311514:31 <br /> Ethyl-tert-butyl ether mg/kg ND 0.25 05/1311514:31 <br /> Ethylbenzene mg/kg NO 0.25 05/13/1514:31 <br /> Methyl-tert-butyl ether mg/kg ND 0.25 05/13115 14:31 <br /> tert-Amylmethyl ether mg/kg ND 0.25 05/13115 14:31 <br /> tert-Butyl Alcohol mg/kg NO 0.25 05113/15 14:31 <br /> Toluene mg/kg NO 0.25 05113/15 14:31 <br /> TPH as Gas mg/kg ND 49.5 05/13/15 14:31 <br /> Xylene(Total) mglkg ND 0.50 05/1311514:31 <br /> 1,2-Dichloroethane-d4(S) °k. 96 70-130 05113/1514:31 <br /> 4-Bromofluorobenzene(S) %. 96 70-130 05/13/15 14:31 <br /> Toluene-d8(S) %. 101 70-130 05113/1514:31 <br /> LABORATORY CONTROL SAMPLE: 208498 <br /> Spike LCS LCS %Rec <br /> Parameter Units Cone. Result %Rao Limits Qualifiers <br /> Benzene mg/kg 2 2.2 109 70-130 <br /> Diisopropyl ether mg/kg 2 2.2 113 70-130 <br /> Ethyl-tert-butyl ether mg/kg 2 2.1 106 65-130 <br /> Ethylbenzene mg/kg 2 2.2 109 70-130 <br /> Methyl-tert-butyl ether mg/kg 2 1.9 98 60-130 <br /> tert-Amylmethyl ether mg/kg 2 1.9 97 70-130 <br /> tert-Butyl Alcohol mg/kg 19.8 19.0 96 70-130 <br /> Toluene mg/kg 2 2.2 111 70-130 <br /> Xylene(Total) mg/kg 5.9 6.5 109 70-130 <br /> 1,2-Dichloroethane-d4IS) %. 94 70-130 <br /> 4-Bromofluorobenzene(S) %. 100 70-130 <br /> Toluene-d8(S) %. 101 70-130 <br /> MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 208499 208500 <br /> MS MSD <br /> 1246740001 Spike Spike MS MSD MS MSD %Rec Max <br /> Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual <br /> Benzene mg/kg NO 2 2 2.3 2.2 113 113 70-130 0 25 <br /> Diisopropyl ether mg/kg ND 2 2 2.3 2.3 117 116 70-130 1 25 <br /> Ethyl-tert-butyl ether mg/kg NO 2 2 2.2 2.1 112 108 65-130 4 25 <br /> Ethylbenzene mg/kg ND 2 2 2.2 2.2 111 111 70-130 0 25 <br /> Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Dale:05114/2015 07:20 PM without the written consent of Pace Analytical Services,Inc.. Page 10 of 17 <br />