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• • Pace Analytical Services,Inc. <br /> 2795 Second Street-Suite 300 <br /> (JceAnalyticalo <br /> _ Davis,CA 95618 <br /> w pawlabs.xm (530)297-4800 <br /> QUALITY CONTROL DATA <br /> Project: DIESEL LINE SAMPLING <br /> Pace Project No.: 1246740 <br /> QC Batch: DAVM/1289 Analysis Method: EPA 82608 <br /> QC Batch Method: EPA 5030 Low Analysis Description: 8260 MSV UST <br /> Associated Lab Samples: 1246740002,1246740003 <br /> METHOD BLANK: 207701 Matrix: Solid <br /> Associated Lab Samples: 1246740002,1246740003 <br /> Blank Reporting <br /> Parameter Units Result Limit Analyzed Qualifiers <br /> Benzene mg/kg ND 0.0049 05/11/1521:17 <br /> Diisopropyl ether mg/kg ND 0.0049 05/11115 21:17 <br /> Ethyl-tert-butyl ether mg/kg NO 0.0049 05/11/1521:17 <br /> Ethylbenzene mg/kg ND 0.0049 05/11/1521:17 <br /> Methyl-tert-butyl ether mg/kg NO 0.0049 05/11/1521:17 <br /> tert-Amylmethyl ether mg/kg NO 0.0049 05/11/1521:17 <br /> tert-Butyl Alcohol - mg/kg ND 0.0049 05/11/15 21:17 <br /> Toluene mg/kg NO 0.0049 05/11/1521:17 <br /> TPH as Gas mg/kg ND 0.97 05/11/15 21:17 <br /> Xylene(Total) mg/kg NO 0.0097 05/11/1521:17 <br /> 1,2-Dichloroethane-d4(S) %. 96 70-130 05/11/1521:17 <br /> 4-Bromofiuorobenzene(S) %. 98 70-130 05/11115 21:17 <br /> Toluene-d8 IS) %. 100 70-130 05/11/1521:17 <br /> LABORATORY CONTROL SAMPLE: 207702 <br /> Spike LCS LCS %Rec <br /> Parameter Units Conc. Result %Rec Limits Qualifiers <br /> Benzene mg/kg .039 0.039 99 70-130 <br /> Diisopropyl ether mg/kg .039 0.040 102 70-130 <br /> Ethyl-tert-butyl ether mg/kg .039 0.036 93 70-130 <br /> Ethylbenzene mg/kg .039 0.040 102 70-130 <br /> Methyl-tert-butyl ether mg/kg .039 0.036 91 70-130 <br /> tert-Amylmethyl ether mglkg .039 0.033 85 70130 <br /> tert-Butyl Alcohol mg/kg .39 0.35 91 70-130 <br /> Toluene mg/kg .039 0.040 102 70-130 <br /> Xylene(Total) mg/kg .12 0.12 102 70-130 <br /> 1,2-Dichloroethane-d4(S) °/a. 97 70-130 <br /> 4-Bromofluorobenzene(S) %. 100 70-130 <br /> Toluene-d8(S) %. 101 70-130 <br /> MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 207703 207704 <br /> MS MSD <br /> 1246607011 Spike Spike MS MSD MS MSD %Rec Max <br /> Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual <br /> Benzene mg/kg .039 .039 0.031 0.034 79 85 70-130 8 25 <br /> Diisopropyl ether mg/kg .039 .039 0.029 0.031 73 79 70-130 9 25 <br /> Ethyl-tert-butyl ether mg/kg .039 .039 0.026 0.028 66 71 70-130 9 25 M1 <br /> Ethylbenzene mg/kg .039 .039 0.032 0.035 83 89 70-130 8 25 <br /> Results presented on this page are in the units Indicated by the"Unita'column except where an alternate unit is presented to the rlghl of the result. <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Dale:05/14/2015 07:20 PM without the written consent of Pace Analytical Services,Inc.. Page 12 of 17 <br />