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• Report Number 40 QC Report Matrix Spike/ Matrix Spike Duplicate Date 3/7/2006 Project Name USAP 110 Project Number 10110,42 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov -Recov Diff Limit Limit Benzene 48638-04 <0 50 400 400 404 392 ug/L EPA 82606 311/06 101 981 282 70-130 25 Toluene 48638-04 <0 50 400 400 39 0 382 ug/L EPA 8260B 311106 974 95 5 203 70-130 25 Tert-Butanol 48638-04 <50 200 200 202 202 ug/L EPA 8260B 311106 101 101 0 438 70-130 25 Methyl-t-Butyl Ether48638-04 <0 50 400 400 388 388 ug/L EPA 82606 311106 970 971 00199 70-130 25 Benzene 48642-02 <0 50 400 400 434 41 9 ug/L EPA 8260B 311106 108 105 349 70-130 25 Toluene 48642-02 <0 50 400 400 440 43 0 ug/L EPA 82606 311106 110 107 247 70-130 25 Tert-Butanol 48642-02 <5 0 200 200 202 207 ug/L EPA 8260B 311106 101 104 2 53 70-130 25 Methyl-t-Butyl Ether48642-02 1 6 40 0 400 378 376 ug/L EPA 82606 311106 906 899 0 766 70-130 25 Benzene 48635-01 <0 50 40 0 400 41 1 400 ug/L EPA 82606 319106 103 999 279 70-130 25 Toluene 48635-01 <0 50 40 0 400 39 0 381 ug/L EPA 8260B 311106 976 95 3 241 70-130 25 Tert-Butanol 48635-01 <5 0 200 200 206 205 ug/L EPA 82606 311106 103 102 0 692 70-130 25 Methyl-t-Butyl Ether 48635-01 <0 50 400 400 354 354 ug/L EPA 8260B 3/1/06 886 886 00231 70-130 25 Benzene 48635-06 18 400 400 558 51 3 ug/L EPA 8260B 311106 944 831 127 70-130 25 Toluene 48635-06 073 400 400 394 35 9 ug/L EPA 82606 311106 966 878 946 70-130 25 Tert-Butanol 48635-06 <5 0 200 200 184 175 ug/L EPA 8260B 3/1106 920 877 479 70-130 25 Methyl-t-Butyl Ether 48635-06 069 400 400 38 0 357 ug/L EPA 8260B 3/1106 933 876 636 70-130 25 f KIFF ANALYTICAL, LLC Approved By Joe rt# 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800