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CASTLE ANALYTICAL LABORATORY , <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 Phone: (209)384-2930 <br /> Certificate#2480 Fax: (209)384-1507 <br /> Moore Twining Associates, Inc. Client Project ID: 9C31007 Method: EPA 5030/8260B ' <br /> 2527 Fresno St. Lab Reference Number:0904046 Instrument ID:VARIAN MS <br /> Fresno, CA.93721 Sample Description:Water Prepared: 04-09-09 <br /> Attn:Andrea Seruntine Analyst: C. Cone Analyzed: 04-09-09 , <br /> Matrix Source: 0904045-03 Reported: 04-16-09 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VWMS-4099 <br /> Reporting BLANK Spiking Control %R , <br /> Limit Result Level Spike Limits <br /> ug/L ug/L ug/L %R <br /> COMPOUNDS ' <br /> t-Butyl Alcohol(t-BA) 20.0 ND 75.0 77.6% 27.2-178. <br /> Meth I t-butyl ether MTBE 0.50 ND 2.50 88.4% 59.7-153.0 <br /> Diisopro yl ether(DIPE) 0.50 ND 2.50 105% 72.1 -129.6 <br /> Eth I t-But I ether ETBE) 0.50 ND 2.50 87.2% 68.1 -130.8 ' <br /> t-Am I meth I ether(TAME 0.50 ND 2.50 98.00/ 60.2-137.1 <br /> 1,2-Dichloroethane 1,2-DCA) 0.50 ND 2.50 78.4% 91.2-137.6 <br /> Ethylene dibromide(EDB) 0.50 ND 2.50 89.6% 69.5-128. <br /> 1,1-Dichloroethene 1,1,DCE 0.50 ND 2.50 83.6% 37.2-160.5 ' <br /> Benzene 0.50 ND 2.50 92.0% 82.0-126.4 <br /> Trichloroethene TCE) 0.50 ND 2.50 95.2% 78.2-127.9 <br /> Toluene 0.50 ND 2.50 88.8% 73.2-138.6 <br /> Chlorobenzene 0.50 ND 2.50 106% 83.7-122.8 ' <br /> Surro ate: <br /> Dibromofluoromethane 10.0 102% 10.0 1 99.8% 78.0-133.7 <br /> 1,2-Dichloroethane-d4 10.0 102% 1 10.0 1 97.0% 81.7-125.4 <br /> Toluene-d8 10.0 99.0% 10.0 93.5% 90.3-112.6 , <br /> 4-Bromofluorobenzene 10.0 104% 10.0 102% 88.0-109.8 <br /> Spiking MATRIX MATRIX %R %RPD ' <br /> Level SPIKE SPIKE DUP Limits <br /> ug/L %R %R <br /> COMPOUNDS <br /> It-Butyl Alcohol(t-BA) 75.0 70.1% 64.0% 45.1 -151.2 9.07% , <br /> Methyl t-butyl ether (MTBE) 2.50 84.8% 80.4% 70.9-144.1 5.33% <br /> Diiso ropylether(DIP 2.50 105% 101% 73.6-126.5 3.88% <br /> Ethyl t-Butyl ether ETBE) 2.50 80.4% 86.0% 74.8-128.1 6.73% <br /> t-Amyl meth I ether TAME) 2.50 85.6% 86.4% 62.5-118.6 0.858% ' <br /> 1,2-Dichloroethane 1,2 DCA) 2.50 90.8% 76.0% 85.4-144.6 17.7% <br /> Ethylene dibromide EDB) 2.50 91.2% 80.8% 73.3-125.1 12.1% <br /> 1,1-Dichloroethene(1,1,DCE) 2.50 88.4% 82.4% 43.2-155.4 7.03% <br /> Benzene 2.50 95.6% 96.8% 75.0-135.0 1.25% ' <br /> Trichloroethene(TCE) 2.50 83.6% 84.8% 83.0-127.5 1.43% <br /> Toluene 2.50 90.0% 1 82.8% 70.8-132.8 8.29% <br /> Chlorobenzene 2.50 97.6% 98.0% 80.3-123.9 0.409% <br /> Surrogate: <br /> ' <br /> Dibromofluoromethane 10.0 95.4% 93.8% 81.3-125.3 1.69% <br /> 1,2-Dichloroethane-d4 10.0 91.8% 95.3% 1 80.2-126.9 3.74% <br /> Toluene-d8 10.0 88.2% 88.4% 1 82.6-114.9 0.227% ' <br /> 4-Bromofluorobenzene 10.0 99.4% 97.0% 84.3-109.9 2.44% <br /> APPROVED BY: ' <br /> James C.Ph/Ili s/Laboratory Director or <br /> ClariJ. Cone/LahoratoryManager <br />