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Entech Analytical Labs, Inc. -- 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 ERM-West,Inc-WC Project Number: 0060269 1777 Botellto Drive,Suite 260 Project Name: Del Monte Walnut Creek,CA 94596 Attn: Paul Hausmann - Certificate of Analysis - Data Report Samples Received: 02/28/2007 Sample Collected by: Client - Lab#: 54204-OC6 Sample ID: SB-2-1.0 Matrix: Solid Sample Date: 2/27/2007 9:15 AM VOCs:EPA 8260B Parameter Result Qua] D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch cis-1,2-Dichloroethent ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E cis-1,3-Dichloropropene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Cyclohexanone ND 1.0 40 µg/Kg N/A N/A 3/2/2007 SM3E070302E Dibromochloromethane ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Dibromomethane ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Dichlorodifluoromeths ne ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E - Diisopropyl Ether ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Ethyl Benzene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Freon 113 ND 1.0 10 µg/Kg N/A N/A 3/2/2007 SM3E070302E Hexachlorobutadiene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E lodomethane ND 1.0 10 µg/Kg N/A N/A 3/2/2007 SM3E070302E Isopropanol ND 1.0 100 µg/Kg N/A N/A 3/2/2007 SM3E070302E ]sopropylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E - Methyl-t-butyl Ether ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Methylene Chloride ND 1.0 50 µg/Kg N/A N/A 3/2/2007 SM3E070302E n-Butylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E n-Propylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Naphthalene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E p-lsopropyltoluene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Pentachlomethane ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E sec-Butylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Styrene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E ten-Amyl Methyl Eth,.r ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E tert-Butanol(TBA) ND 1.0 40 µg/Kg N/A N/A 3/2/2007 SM3E070302E tert-Butyl Ethyl Ether ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E tert-Butylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Tetrachloroethene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Tetrahydrofuran ND 1.0 40 µg/Kg N/A N/A 3/2/2007 SM3E070302E Toluene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E trans-l,2-Dichloroeth,;ne ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E trans-l,3-Dichloropro)ene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E trans-l,4-Dichloro-2-Butene ND 1.0 10 µg/Kg N/A N/A 3/2/2007 SM3E070302E Trichloroethene ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Trichlorofluoromethane ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Vinyl Acetate ND 1.0 5.0 µg[Kg N/A N/A 3/2/2007 SM3E070302E Vinyl Chloride ND 1.0 5.0 µg/Kg N/A N/A 3/2/2007 SM3E070302E Xylenes,Total ND 1.0 10 µg/Kg N/A N/A 32/2007 SM3E070302E Surrogate Surrogate Recovery Control Limits(%) 'Analyzed by: Mfelix 4-Bromofluoroben::ene 90.0 60 130 Reviewed by: Eric Kum Dibromofluoromet Lane 94.9 60 - 130 Toluene-d8 101 60 130 Detection Limit=Dejection Limit for Reporting. ND=Not Detected at or above the Detection Limit. D/P-F=Dilution and,or Prep Factor includes sample volume adjustments. Qua]=Data Qualifier 3 7,'2007 6:55:10 PM-ECumiffe