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Entech Analvtical Labs, Inc. `' r <br /> 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 <br /> ERM-West,Inc-WC Project Number: 0060269 <br /> 1777 Botelao Drive,Suite 260 <br /> Project Name: Del Monte <br /> Walnut Creek,CA 94596 <br /> Attn: Paul Hausmann <br /> Certificate of Analysis - Data Report Samples Received: 02/28/2007 <br /> Sample Collected by: Client <br /> Lab#: 54204-0:0 Sample ID: SB-4-20 Matrix: Solid Sample Date: 2/27/2007 11:36 AM <br /> VOCs:EPA 8260B <br /> Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch <br /> cis-1,2-Dichloroethenc ND LO 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> cis-1,3-Dichloropropene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Cyclohexanone ND 1.0 40 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Dibromochloromethane ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO703056 <br /> Dibromomethane ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Dichlorodifluorometha ne ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Diisopropyl Ether ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Ethyl Benzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Freon 113 ND 1.0 10 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Flexachlorobutadiene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> lodomethane ND 1.0 10 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Isopropanol ND 1.0 100 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> lsopropylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Methyl-t-butyl Ether ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Methylene Chloride ND 1.0 50 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> n-Butylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> n-Propylbenzene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Naphthalene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> p-Isopropyltoluene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Pentachloroethane ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> sec-Butylbenzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Styrene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> tert-Amyl Methyl Ethc r ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> tert-Butanol(TBA) ND LO 40 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> tert-Butyl Ethyl Ether ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> tert-Butylbenzene ND LO 5.0 ttg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Tetrachloroethene ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6GO703050 <br /> Tetrahydrofiran ND LO 40 gg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Toluene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM60070305G <br /> trans-1,2-Dichloroethtne ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> trans-1,3-Dichloroprotene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> trans-l,4-Dichloro-2-butene ND 1.0 10 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Trichloroethene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Trichlorofluoromethwie ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Vinyl Acetate ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Vinyl Chloride ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Xylenes,Total ND 1.0 10 µg/Kg N/A N/A 3/5/2007 SM6GO70305G <br /> Surrogate Surrogate Recovery Control Limits(%) Analyzed by: EricKum <br /> 4-Bromofluorobem ene 94.2 60 130 Reviewed by: mfelix <br /> Dibromofluorometllane 124 60 130 <br /> Toluene-d8 94.6 60 130 <br /> Detection Limit=Detaction Limit for Reporting. ND=Not Detected at or above the Detection Limit. <br /> F)/P-P=Dilution ands it Pren Factor inchides samnle volume adiustments. Oual=Data Oualifier 3.72007 6:55:11 PM•ECunniffe <br />