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Entech Analytical Labs, Inc. 3334 Victor Court , .Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 1 ERM-West,Inc-WC Project Number: 0060269 J 1777 Botelho Drive,Suite 260 Project Name: Del Monte Walnut Creek,CA 94596 Attn: Paul Hausmann Certificate of Analysis -Data Report Samples Received: 02/28/2007 Sample Collected by: Client Lab#: 54204-021 Sample ID: SB-5-1.0 Matrix: Solid Sample Date: 2/27/2007 12:11 PM VOCs:EPA 8260B Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch cis-1,2-Dichlorcethenu ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G cis-1,3-Dichloropropene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6G070305G Cyclobexanone ND 1.0 40 pg/Kg N/A N/A 3/5/2007 SM6G070305G Dibromochloromethane ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6G070305G t Dibromomethane ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6G070305G J Dichlorodifluoromethane ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Diisopropyl Ether ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6G070305G Ethyl Benzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Freon 113 ND 1.0 10 pg/Kg N/A N/A 3/5/2007 SM6G070305G Hexachlorobutadiene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6Go70305G lodomethane ND 1.0 10 pg/Kg N/A N/A 3/5/2007 SM6G070305G f Isopropanol ND 1.0 100 gg/Kg N/A N/A 3/5/2007 SM6G070305G �JJ Isopropylbenzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Methyl-t-butyl Ether ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Methylene Chloride ND 1.0 50 pg/Kg N/A N/A 3/5/2007 SM6G070305G n-Butylbenzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G n-Propylbenzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Naphthalene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G y p-Isopropyltoluene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G J Pentachlomethane ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G sec-Butylbenzene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Styrene ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6G070305G tert-Amyl Methyl Eth(a ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G tert-Butanol(TBA) ND 1.0 40 gg/Kg N/A N/A 3/5/2007 SM6G070305G tert-Butyl Ethyl Ether ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6G070305G Cert-Butylbenzene ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6G070305G Tetrachloroethene ND 1.0 5.0 µg/Kg N/A N/A 3/5/2007 SM6G070305G Tetrahydrofuran ND 1.0 40 µg/Kg N/A N/A 3/5/2007 SM6G070305G Toluene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G trans-1,2-Dichloroethcne ND loo 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G trans-l,3-Dichloropropene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G trans-l,4-Dichloro-2-butene ND 1.0 10 pg/Kg N/A N/A 3/5/2007 SM6G070305G Trichloroethene ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6G070305G Trichlorofluoromethane ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6Go70305G Vinyl Acetate ND 1.0 5.0 gg/Kg N/A N/A 3/5/2007 SM6G070305G Vinyl Chloride ND 1.0 5.0 pg/Kg N/A N/A 3/5/2007 SM6Go70305G Xylenes,Total ND 1.0 10 pg/Kg N/A N/A 3/5/2007 SM6G070305G Surrogate Surrogate Recovery Control Limits(%) .Analyzed by: EricKum 4-Bromofluoroben7 ene 94.3 60 - 130 Reviewed by: mfelix i Dibromofluoromethane 125 60 - 130 J Toluene-d8 102 60 - 130 Detection Limit=Detection Limit for Reporting. ND=Not Detected at or above the Detection Limit. f DLP-F=Dilution and/)r Prep Factor includes sample volume adjustments. Qual=Data Qualifier 3/7/2007 6:55:12 PM-ECu iRe J