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Sequoia los, A 94070-4111 <br /> 40701 Road <br /> San Carlos,CA 94070-41 1 1 <br /> 1 (650) 232-9600 <br /> IWO Analytical i FAX(650) 232-9612 <br /> Gettler-Ryan/Geostrategies(1) Project Unocal(1) s" Sampled 11/23/99 <br /> 6747 Sierra Court,Suite D Project Number Unocal SSO187/Job#280045, Received 11/24/99 <br /> Dublin,CA 94568 Project Manager Deanna Hardin&___,_ Reported 12/10/99 <br /> Sample Description , U-2 <br /> Laboratory Sample Number L911275-03 <br /> Batch Date Date Specific Method/ Reporting <br /> IAnalyte Number Prepared Analyzed Surrogate Limits Limit Result Units Notes* <br /> Sequoia Analytical-San Carlos <br /> Total Puraeable Hydrocarbons(C6-C12),BTEX and MTBE by DHS LUFT <br /> Purgeable Hydrocarbons as Gasoline 9120017 12/3/99 1213/99 50 0 ND ug/I <br /> Benzene " to " 0 500 ND It <br /> Toluene " to " 0 500 ND It <br /> Ethylbenzene to1' 0 500 ND it <br /> Xylenes(total) " of " 0 500 ND 1,11 <br /> Methyl tert-butyl ether of1' 500 ND " <br /> Surrogate a,a a-Triuorotoluene ;' ' ' ' ti ' 70 0-130 821 <br /> Volatile Organic Oxygenated Compounds by EPA Method 8260A <br /> Ethanol 9120020 1215/99 12/6/99 1000 ND ug/E <br /> Teri-butyl alcohol ". 200 ND " <br /> Methyl tert-butyl ether _ ,y 200, - ND <br /> Di-isopropyl ether 200 ND m <br /> Ethyl ter[-butyl ether 200 ND " <br /> Tert-amyl methyl ether _ "_ " 200 ND " <br /> Surrogate 1 2-Dichloroerhane-d4 760-114 105 <br /> f <br /> 1 <br /> t <br /> i <br /> Sequoia Analytical-San Carlos *Refer to end of report for text of notes and defrnettons <br /> Page 4 of 28 <br />