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110 2nd Avenue South,#137,Pacheco,CA 945 53-5 560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 niccatti <br /> } llwwry nbell com E-mail main@mccampbell com <br /> Environmental Science Associates Client Project ID #UOP 20025 2 Date Sampled 01/10-01/11/01 <br /> 225 Bush Street,Suite 1700 Date Received 01/12/01 <br /> Client Contact Peter Hudson Date Extracted 01/12/01 <br /> San Francisco,CA 94104 <br /> Client P O Date Analyzed 01/16/01 <br /> Lead* <br /> EPA analytical methods$0101200 7,239 2` <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 57778 5-14-TPIA S TTLC 77 102 <br /> 57779 5-14-TP5A S TTLC 59 I00 <br /> 57780 5-14-TP4A S TTLC 88 98 <br /> 57781 5-14-TP14 S TTLC 60 102 <br /> 57782 5-14-TP10 S TTLC 67 106 <br /> 57783 5-14-TP15 S TTLC 78 103 <br /> S TTLC 3 0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated,ND means not detected above W TTLC 0 005 mg/L <br /> the reporting limit <br /> -- STLC,TCLP 0 2 mg/L <br /> 'soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water samples and all STLC/SPLP/TCLP extracts in mg/L <br /> 'Lead is analysed using EPA method 6010(ICP)for soils,sludges, STLC & TCLP extracts and method 239 2 (AA Furnace) for water <br /> samples <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(orgamc matrices,TTLC),3050(solids,TTLC),STLC-CA Title 22 <br /> "surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> °reporting limit raised due matrix interference <br /> . i) liquid sample that contains greater than --2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />