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1 925 798 4�it2;enc, ; Feb-11 -02 1 :43FM; Page 5(6 <br /> • -- - - - — <br /> Sent By: McCampbell Analyticals <br /> [W 2nd Avenue South,#D7,Facheta,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC, Teiephone:915-798-1620 Fax :925-798-1522 <br /> l t W%vwW.rnceam bcll.com E-mail: main@-i)mecampbell.cum <br /> Advanced GeoEnvironmentai Client Project ID: Sho.;key&Sons ! Date Sampled:01/29,102 <br /> 837 Shaw Road Trucking Date Received: 01/30/02 <br /> Stockton,CA 9521$ Client Contact:Bill Lit Date Extracted:02/04-02/08/02 , <br /> Client P.O-. Date Analyzed: 02/04-02/08102 <br /> Oxygenated Volatile U rganics By GUMS <br /> IrYA method 8260 modified <br /> Lab ID 89275 89216 89277 89278 <br /> MW_it MW 2/ MW-3/ MW-4/ <br /> 01-29-02 <br /> Client ID 01-29-02 01-29.02 01-29-02 01.29-02 <br /> Matrix W W W W 5 W <br /> Compound C oncentranon* ug/kg uglL <br /> Di-isopropyl Ether(T)IFE) ND NO Nth ND<5.0 5.0 1.0 <br /> Ethyl tort-Buryt Ether(ETRE) ND N'D Nth ND<5.0 5.0 1 A <br /> Methyl-tort Butyl Enter(Mini) ND ND ND ND<5.0 S.o 1.o <br /> 10 Cert-Arnyt Methyl Ether(TAME) ND ND ND ND<5_@ 5.0 1.0 <br /> tert Butanal ND ND ND Nr)<25 25 5.0 <br /> Surrogate Recover ies <br /> nibromolluoromethane 107 103 105 106 <br /> ' Comments: h <br /> water samples are rcported itt uglL.,sotit end sludge samples in ug�kg,wipe< in ug/wipe and all TCU i STLC/SPLP extracts in ug?L <br /> ND means not detected above the reporting limit;NIA means surrogate not A pticable to this analysis <br /> (h)lighter than water irttnusi;Mr sheen is present;(i)liquid sample that cum Sins greater thult­5 rot.%sediment;b)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />