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110 2nd Avenue South, #D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Tele-510-798-1620 Fax:510-798-1622 I <br /> j <br />'r Advanced GeoEnvironmental,Inc. Client Project ID: Shockey & Sons Date Sampled:09/24/96 <br /> 1803 West March Lane, Suite A Trucking <br /> Date Received:09/25/96 j <br /> Stockton,CA 95207 Client Contact: Bill Little Date Extracted: 09128-09130196 <br /> Client P.O: Date Analyzed:09128-09/30/96 <br /> Gasoline Range(C6-C12) Volatile Hydrocarbons as Gasoline*,"ith Methyl tert-Butyl Ether* &BTEX* <br /> EPA methods 5030modified 8015 and 8020 or 601California RW CB SF Ba Re ion method GCFID(5030 <br /> Lab ID Client ID MatrixTPH(g)+ MTBE Benzene Toluene Ethylben- Xylenes %Rec. <br />' zene Surrogate <br /> 69445 MW1/9-24-96 W 730,g,h ND 0.75 1.9 0.94 50 95 <br />' 69446 MW2/9-24-96 W ND ND ND ND ND ND 102 <br /> 69447 MW3/9-24-96 W ND ND ND ND ND ND 103 <br /> 69448 M W 4/9-24-96 W --- ND< 10 10 2.2 4.1 12 94 <br /> I <br /> i <br />' Reporting Limit unless W 50 ug/L 5.0 0.50,5 0.5 0.5 <br /> otherwise stated;ND <br /> means not detected <br /> above the reporting limit S 1.0 mg/kg 0.05 0.005 0.005 0.005 0.005 <br />' *water and vapor samples are reported in ug/L,soil and sludge samples in mg/kg,and all TCLP ex1racts in mg/L <br /> #cluttered chromatogram;sample peak coelutes iwith surrogate peak <br />' + The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not <br /> responsible for their interpretation:a) unmodified or weakly modified gasoline is siTnifcant;b) hearzergasoline <br /> range compounds are siggnn�cant(aged gasoline?);c)lightergasoline range compounds(the most mobile 1Faction) <br /> I' are significant; d) asorne range compounds having broad chromatographic peaks are significant; biologically <br /> altered gasoline?;e� TPH pattern that does not appear to be derived from gasoline (?); f) one to a few isolated <br /> peaks present;g)strongly aged gasoline or diesel range compounds are significant;h)lighter than water immiscible <br /> /o <br /> sheen is present; i) Iiquid sample that contains greater than_ 5 vol. sediment;j) no recognizable pattern. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />