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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' h //www mccam bell com E-mail mam@mccampbell com <br /> I <br /> Advanced GeoEnvironmental Client Project ID Chet's Auto Date Sampled 10/23-24/01 <br /> 837 Shaw Road Date Received 10/25/01 <br /> 1 Stockton, CA 95215 Client Contact Bill Little Date Extracted 10/25/01 <br /> Client P G Date Analyzed 10/30-10/31/01 <br /> Volatile Organics By GCIMS <br /> i EPA method 8260 <br /> ' Lab ID 82007 <br /> Client ID B3-40 <br /> Matrix S <br /> Compound Concentration* 4Rgp=4� <br /> Compound Concentration* Reporting Urn t W S <br /> Acetone 1b) ND<50 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 so <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 so <br /> Bromochloromethane ND 10 5 0 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND 10 50 <br /> Bromotorm ND 10 50 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone t ND 10 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride"i ND<15 10 50 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 1 10 <br /> Carbon Disulfde ND l 0 50 Methyl isobutyl ketone 191 ND 1 0 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 1� . 5 0 Naphthalene ND 5 0 5 0 <br /> Chloroethane ND 50 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether` ND 5 0 Styrene ND 1 0 5 0 <br /> Chloroform ND 5 0 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 50 1,1,2,2-Tetrachloroethane ND to 5 0 <br /> 2-Chlorotoluene ND 5 0 Tetrachloroethene ND 10 50 <br /> 1 4-Chlorotoluene ND 50 Toluene ND 10 50 <br /> Dibromochloromethane ND 5 0 1,2,3-Tnchlorobenzene ND 50 25 <br /> 12 Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2 Trichloroethane ND 1 0 5 0 <br /> 1 3-Dichlorobenzene ND 10 50 Trichloroethene ND to 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2 3-Tnchloropropane ND 10 50 <br /> 1,1 Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 1 0 5 0 <br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate m ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride ° ND 1 0 5 0 <br /> ' trans-l,2-Dichloroethene ND 10 5 0 Xylenes,total ND ] 0 5 0 <br /> 1 2-Dichloropropane ND to 50 Comments <br /> 1,3-Dichloropmpane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichlorapropane ND 10 50 Dibromofluaromethane 90 <br /> 1,I-Dichloropropene ND 10 50 Toluene-d8 105 <br /> cis-1,3-Dichloropropene ND 10 1 50 4-BromofluorobenzeneL7)17 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/Ape and all TCLP/SPLP extracts in ug/L, <br /> ' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (0 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than --5 vol % <br /> sediment, {1) sample diluted due to high organic content, (k) ethenylbenzene, (1) methyibenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />