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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmentalClient Project FD Chefs Auto Date Sampled 10/23-24/01 <br /> $37 Shaw Road Date Received 10/25/01 <br /> Stockton, CA 95215 Client Contact Bill Little Date Extracted 10/25/01 <br /> 1 <br /> ' Client P O Date Analyzed 10/29/01 <br /> LUF'T Metals* i <br /> EPA analytical methods 6010/200 7,239 2* <br /> Lab ID Client ID Matrix Extraction'177 <br /> ickel ZInC %Recovery <br /> Surrogate <br /> 81995 B 1-10' S TTLC40 67 103 <br /> 81996 B1-20' S TTLC40 160 102 <br /> 81997 81-25' S TTLC6 57 102 <br /> g81999 <br /> B1-30 S TTLC ND4 69 101 <br /> B1-40 S TTLC ND 29 47 25 49 106 <br /> $2000 B1-50 S TTLC ND 25 70 19 53 102 <br /> 82001 BI-60 S TTLC ND 9 8 ND 72 39 106 <br /> 82002 B2-20 S TTLC ND 46 <br /> 64 44 70 101 <br /> 82005 B3-20 S TTLC ND 27 4 8 35 45 101 <br /> Reporting Limit unless $ TTLC O S mg/kg 05 30 2 0 ;p <br /> otherwise stated ND <br /> means not detected above `� TTLC 0 005 mg/L 0 02 0 005 0 05 0 OS <br /> the reporting limit _ STLC, <br /> 1TCLP 0 01 mg/L 005 02 003 005 <br /> *water samples are reported in mg/L soil and sludge samples in mg/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts m mglL <br /> °Lead is analysed using EPA method 6010(ICP)for soils,STLC&TCLP extracts and method 239 2(AA Fumace)for water samples <br /> EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,,rTLC),3050(solids,TTLC),STLC-CA Title 22 <br /> DISTLC extractions are performed using STLC methodology except that deionized water is substituted for citric acid buffer as the <br /> extraction fluid DISTLC results are not applicable to STLC regulatory limits <br /> ' s surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> &reporting limit raised due to matrix interference <br /> i) liquid sample that contains greater than —2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> ' methodologies and can significantly effect reported metal concentrations <br /> DHS Certification No 1644 <br /> Edward Hamilton,Lab Director <br />