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I 10 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> hM://www,mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Chapin Brothers Date Sampled: 03/30/99 <br /> 4005 North Wilson Way Date Received: 03/31/99 <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 04/03-04/05/99 <br /> [Client P.O: Date Analyzed: 04/03-04/05/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> LablD 08263 08265 08267 08269 <br /> Reporting Limit <br /> Client ID MWI/3-30-99 MW5/3-30-99 MW3/3-30-99 VE-6 <br /> Matrix W W W W S W <br /> �- Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND 47 74 54 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND<6 5.0 1A <br /> Methyl-tert Butyl Ether(MTBE) 2.3 ND ND ND<6 5.0 1.0 <br /> ,. tert-Amyl Methyl Ether(TAME) ND ND ND ND<6 5.0 1.0 <br /> tert-Butanol ND ND ND ND<30 25 5.0 <br /> Surrogate Recoveries <br /> Dibromofluoromethane 95 94 97 98 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in uglkg,ahpes in ugl"ipe and all TCLP 1 STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 �,A Edward Hamilton,Lab Director <br />