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CHAPTER 5 <br /> SITE CLOSURE ACTiVJTIES <br /> 111 <br /> } As discussed in Chapter 3, the soil was demonstrated to be nonhazardous and the <br /> hydrocarbons to be nonleachable. As7wel-, the lack of destruction of- the hydrocarbons`by- <br /> obioreinediatior , -as discussed in Chapter 4, further demonstrates the stability of the long chain <br /> hydrocarbons `and the unlikelihood of their mobility: Therefore, Brown and Caldwell (BC) <br /> recommended that the excavation be backfilled with the soil (Attachment F). Prior to backfilling, <br /> { BC recommended collecting additional soil samples to document the amount of petroleum <br /> hydrocarbon in the soil to be left in place. The County verbally agreed with this recommendation <br /> } and the specific site closure activities occurred. The 1993 work conducted by BC was done in <br /> accordance with the Site Safety and Health Plan included as Attachment H. <br /> I <br /> Once the physical limits of the excavation had been reached, 10 confirmation soil <br /> samples were collected from the sidewalls and bottom of the excavation. The samples were <br /> collected by BC on September 20, 1993, under the direct supervision of the San Joaquin County <br /> Public Health Services Department (County), at locations mutually agreed upon by BC and the <br /> County. Sampling followed the procedures outlined in the September 3, 1993, BC Status Report <br /> for Kent's Oil Remediation Project, included in Attachment F. The samples were analyzed for <br /> total petroleum hydrocarbons as diesel (TPHd) and total petroleum hydrocarbons as motor oil <br /> (TPHmo) following the procedures outlined above. Samples were also analyzed for TPHd and <br /> TPHmo following the toxicity characteristic leaching procedure (TCLP) (EPA Method 1310). <br /> TPHd and TPHmo were identified in one of the 10 confirmation samples collected from the <br /> excavation at concentrations of 37 milligrams per kilogram (mg/Kg) and 38 mg/Kg, respectively. I <br /> e However, the results of the 10 confirmation samples analyzed for TPHd and TPHmo following <br /> the TCLP method indicated that these petroleum hydrocarbons were not leachable from the soil. <br /> The locations of the confirmation samples are shown on Figure 5-1, and Table 5-1 presents the <br /> analytical results. <br /> 3 <br /> On September 20, 1993, BC also collected under the supervision <br /> of the County, 32 soil <br /> samples from the stockpiled material for laboratory analysis. The samples were composited by <br />{ the analytical laboratory at a ratio of 2 to 1 and the resulting 16 composite samples were <br /> analyzed for the presence of TPHd and TPHmo, following the TCLP procedures described above. <br /> In addition, five of the composite samples were also analyzed for TPHd and TPHmo following <br /> EPA Method 8015 modified. Analytical results of the EPA 8015 modified analysis identified <br /> TPHd and TPHmo concentrations ranging from 180 mg/kg to 2100 mg/kg, and 480 mg/kg to <br /> 3600 mg/kg, respectively. Results of the TCLP analysis indicated that the TPHd and TPHmo <br /> identified in the soil is not leachable. Table 5-2 summarizes the results of the stockpile <br /> confirmation soil samples. The complete laboratory reports and chain-of-custody documentation <br /> l <br /> Use or disclosure of data contained on this sheet is subject to the restriction specified at the beginning of this doctunent. <br /> 12n Z9 SIC\760M M10RTSKEYr-0ILCLO <br /> Q�1SPSi00 <br /> F <br />