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A <br /> Volatile Hydrocarbons by GOMS in Water <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch B001184-EPA 5030 GC/MS <br /> Blank(B001184-BLKI) Prepared 06/20/06 Analyzed 06121/06___ <br /> Benzene ND 050 ltg/L <br /> Toluene ND 050 lµg/L <br /> Ethylbenzene ND 050 gg/L <br /> m,p-Xylene ND 050 µg/L <br /> o-Xylene ND 050 pg/L <br /> Ethanol ND 250 pg/L <br /> Tertiary Butyl Alcohol (TBA) ND 12 pg/L <br /> Methyl tert-Butyl Ether (MTBE) ND 10 µg/L <br /> Di-isopropyl Ether (RIPE) ND 10 µg/L <br /> Ethyl tert-Butyl Ether (ETRE) ND 10 pg/L <br /> Tert-Amyl Methyl Ether (TAME) ND 10 µg/L <br /> Surrogate Dibromofluoromethane 201 legIL 200 100 70-130 <br /> Surrogate Toluene-d8 205 UgIL 200 102 70-130 <br /> Surrogate 4-Bromofluorobenzene 200 leg/L 200 100 70-130 <br /> Matrix Spike 001184-MS1 Source 6061610-05 Prepared 06/20/06 Analyzed 06/21/06 <br /> 1,1-Dichloroethene(1,1-D CE) 23 2 1 0 µg/L 250 ND 93 70-130 <br /> Benzene 23 7 050 µg/L 25 0 ND 95 70-130 <br /> Trichloroethene(TCE) 242 10 ltg/L 250 ND 97 70-130 <br /> Toluene 247 050 µg/L 25 0 ND 99 70-130 <br /> Chlorobenzene 239 10 µg/l- 25 0 ND 96 70-130 <br /> Surrogate Debromofluoromelhane 205 UgIL 200 102 70-130 <br /> Surrogate Toluene-d8 202 ,uglL 200 101 70-130 <br /> Surrogate 4-Bromofluorobenzene 203 UgIL 200 102 70-130 <br /> Matrix S tke Du B001184-MSD1 Source 6061610-05 Prepared 06/20/06 Analyzed 06/21/06 <br /> I,1-Dichloroethene(l,l-DCE) 23 4 10 }rg/L 250 ND 94 70-130 1 20 <br /> Benzene 244 050 gg/L 25 0 ND 98 70-130 3 20 <br /> Trichloroethene(TCE) 246 10 }µg/L 250 ND 98 70-130 1 20 <br /> Toluene 256 050 µg/L 25 0 ND 102 70-130 3 20 <br /> Chlorobenzene 242 1 0 ltg/L 250 ND 97 70-130 1 20 <br /> Surrogate Dtbromofluoromethane 204 pgIL 200 102 70-130 <br /> Surrogate Toluene-d8 204 NgIL 200 102 70-130 <br /> Surrogate 4-Br omofluorobenzene 200 UgIL 200 100 70-130 <br /> • Page 13 of 14 <br /> I ah Project# 6061610 CA Lab Accreditation# 2303 <br />