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GEL LABORATORIES LLC <br /> 2040 Savage Road Charleston SC 29407-(843)556-8171 -www.gal.com <br /> Certificate of Analysis <br /> Report Date: November 23,2016 <br /> Company: Lawrence Livermore National Security,LLC <br /> Address: 7000 East Avenue <br /> MailStop L-620 <br /> Livermore,California 94551 <br /> Contact: Mr.Chad F.Davis <br /> Project: RHWM WSAP-Normal Deliverable <br /> Client Sample ID: W356456 Project: LLNL00301 <br /> Sample ID: 410337002 Client 1D: LLNL003 <br /> Parameter Qualifier Result DL RL Units PF DF Analyst Date_ Time Batch Method <br /> Volatile Organics <br /> GEL 8260B Method List Soil(W8260)"As Received" <br /> Vinyl acetate-8885 U ND 167 500 ug/kg 2.00 50 <br /> Vinyl chloride-8900 U ND 33 3 100 ug/kg 2.00 50 <br /> Xylenes(total)-8975 U ND 100 300 ug/kg 200 50 <br /> cis-1,2-Dichloruclhylcne-3695 U ND 333 IN ug/kg 200 50 <br /> cis-1,3-Dichloropropylene-3900 U ND 33.3 100 ug/kg 200 50 <br /> m,p-Xylenes-8980 U ND 667 200 ug/kg 200 50 <br /> n-Butylbenzenc-5830 U ND 33 3 100 uglkg 2.00 50 <br /> n-Propylbcazcnc-5835 U ND 33.3 100 ug/kg 2.00 50 <br /> o-Xylenc-6275 U ND 33.3 100 ug/kg 2.00 50 <br /> scc-Butylbenzene-7575 U ND 33.3 100 uglkg 2.00 50 <br /> tert-Burylbenzene-8180 U ND 33.3 100 ug/kg 2.00 50 <br /> trans-1,2-Dichloroethylene-3700 U ND 33.3 100 ug/kg 2.00 50 <br /> trans-l,3-Dichloro propyIcne-3950 U ND 33.3 100 ug/kg 2.00 50 <br /> trans-l,4-DichIoru-2-butcoc-3286 U ND 167 500 uglkg 2.00 50 <br /> The followin Pre Methods wereperformed: <br /> Method Description Analyst Date Time Prep Batch <br /> SW946 5030 volutle 5030 Solid Prep VXYI 11.17/16 1016 1617291 <br /> The following Analytical Methods were performed: <br /> Method Descri don _ Analyst Comments <br /> I SW846 82608 <br /> Surrogate/Tracer Recovery Test _Result Nominal Recovery% Acceptable Limits <br /> 1,2-Dichloroethane-d4.3601 GEL 8260B Method List Soil(W8260)"As 4700 uglkg 50.0 94 (810/W24%) <br /> Received" <br /> Bromonuorobcnzene-1420 GEL 9260B Method List Soil(W8260)`As 4910 ug/kg 50.0 98 (70°/x130%) <br /> Received" <br /> Toluene-d8.8351 GEL 82608 Method List Soil(W8260)"As 4880 ug/kg 50.0 98 (81°a 120%) <br /> Received" <br /> Notes: <br /> age 18 of 56 <br />