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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Pax:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 Report Number: IU11062 Received: 09/13/11 <br /> Attention: Lorin King <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit MDL Result Factor Extracted .Analyzed Qualifiers <br /> Sample ID:IU11062-31 (MW-35-Water) Sampled:09/08/11 <br /> Reporting Units: ug/I <br /> Benzene EPA 8260E 1111493 0.50 0.28 ND 1 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111493 0.50 0.25 ND 1 9/14/2011 9/15/2011 <br /> Toluene EPA 82608 1111493 0.50 0.36 ND 1 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 82608 1111493 1.0 0.90 ND 1 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 8260B 1111493 1.0 0.25 ND 1 9/14/2011 9/15/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 82608 6111493 1.0 0.32 ND 1 9/142011 9/15/2011 <br /> ten-Butanol(TBA) EPA 8260B 1111493 10 6.5 ND 1 9/14/2011 9/15/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-12091o) 93% <br /> Surrogate:Dibromofluoromethane(80-120%) 111 % <br /> Surrogate: Toluene-d8(80-12001o) 97% <br /> Sample ID: IU11062-32(MW-36-Water) Sampled: 09/08/11 <br /> Reporting Units: ug/1 <br /> Benzene EPA 82608 1111493 0.50 0.28 ND 1 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 8260B 1111493 0.50 0.25 ND 1 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111493 0.50 0.36 ND 1 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 8260B 1111493 1.0 0.90 ND 1 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1111493 1.0 0.25 ND 1 9/14/2011 9/15/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 1111493 1.0 0.28 ND 1 9/142011 9/15/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1111493 1.0 0.32 ND 1 9/14/2011 9/15/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 82608 1111493 1.0 0.33 ND 1 9/14/2011 9/152011 <br /> tert-Butanol(TBA) EPA 82608 1111493 10 6.5 ND 1 9/14/2011 9/15/2011 <br /> Ethanol EPA 8260B 1111493 150 100 ND 1 9/142011 9/15/2011 <br /> Surrogate: 4-Bromofluorobenzene(80-120%) 92% <br /> Surrogate.'Dibromofluoromethane(80-12091o) 112% <br /> Surrogate: Toluene-d8(80-120016) 95% <br /> Sample ID: W11062-33(MW-37-Water) Sampled: 09/09/11 <br /> Reporting Units: ug/1 <br /> Benzene EPA 82608 1111489 2.5 1.4 320 5 9/14/2011 9/15/2011 <br /> Ethylbenzene EPA 82608 1111489 2.5 1.2 7.3 5 9/14/2011 9/15/2011 <br /> Toluene EPA 8260B 1111489 2.5 1.8 13 5 9/14/2011 9/15/2011 <br /> Xylenes,Total EPA 82608 1111489 5.0 4.5 28 5 9/14/2011 9/15/2011 <br /> Di-isopropyl Ether(DIPE) EPA 82608 1111489 5.0 1.2 57 5 9/142011 9/15/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 1111489 5.0 1.4 ND 5 9/14/2011 9/15/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 1111489 5.0 1.6 590 5 9/14/2011 9/15/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 1111489 5.0 1.6 1.6 5 9/14/2011 9/15/2011 1 <br /> Cert-Butanol(TBA) EPA 8260B 1111489 50 32 3000 5 9/142011 9/15/2011 <br /> Surrogate:4-Bromofluorobenzene(80-120%) 100% <br /> Surrogate:Dibromofluoromethane(80-120%) 103% <br /> Surrogate: Toluene-d8(80-120%) 105% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report.shall not be reproduced, <br /> except in full,without written permiseton from TestAmerica. 1 U11062 <page 25 Of 67> <br />