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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite loo. Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Blaine Tech San Jose/CRA Shell Project ID: 3515 Nary Dr.,Stockton,CA <br /> 1680 Rogers Avenue Sampled: 09/07/11-09/09/11 <br /> San Jose,CA 95112-1105 Re ort Number: IU11062 <br /> Attention: Lorin King p Received: 09/13/11 <br /> METHOD BLANK/QC DATA <br /> VOLATILE ORGANICS by GC/MS (EPA 5030B/8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch: 1111329 Extracted: 09/13/11 <br /> LCS Analyzed:09/13/2011 (1111329-BSI) <br /> Di-isopropyl Ether(DIPE) 23.8 1.0 ug/I 25.0 95 60-135 <br /> Methyl-tert-butyl Ether(MTBE) 23.1 1.0 ug/I 25.0 92 60-135 <br /> Methyl-tert-butyl Ether(MTBE) 23.1 1.0 ug/I 25.0 92 60-135 <br /> tert-Butanol(TBA) 138 10 ug/l 125 110 70-135 <br /> Surrogate:4-Bromofluorobenzene 24.7 119/1 25.0 99 80-120 <br /> Surrogate:4-Bromofluorobenzene 24.7 49/1 25.0 99 80-120 <br /> Surrogate:Dibromofluoromethane 23.8 ug/1 25.0 95 80-120 <br /> Surrogate:Dibromofluoromethane 23.8 ug/1 15.0 95 80-120 <br /> Surrogate:Toluene-d8 14.8 u9/1 25.0 99 80-120 <br /> Surrogate:Toluene-d8 24.8 ug// 25.0 99 80-120 <br /> Matrix Spike Analyzed:09/13/2011 (1111329-MSI) Source: IUI0857-01 <br /> Benzene 23.2 0.50 ug/I 25.0 ND 93 65-125 <br /> Benzene 23.2 0.50 ugfl 25.0 ND 93 65-125 <br /> Ethylbenzene 26.2 0.50 ug/I 25.0 ND 105 65-130 <br /> Ethylbenzene 26.2 0.50 ug/I 25.0 ND 105 65-130 <br /> Toluene 25.4 0.50 ugA 25.0 ND 102 70-125 <br /> Toluene 25.4 0.50 ugA 25.0 ND 102 70-125 <br /> m,p-Xylenes 52.5 1.0 ugfl 50.0 ND 105 65-130 <br /> m,p-Xylenes 52.5 1.0 ugA 50.0 ND 105 65-130 <br /> o-Xylene 25.9 0.50 ug/I 25.0 ND 103 65-125 <br /> o-Xylene 25.9 0.50 ugA 25.0 ND 103 65-125 <br /> Xylenes,Total 78.4 1.0 ugA 75.0 ND 105 60-130 <br /> Xylenes,Total 78.4 1.0 ugA 75.0 ND 105 60-130 <br /> Di-isopropyl Ether(DIPE) 22.2 1.0 ugA 25.0 ND 89 60-140 <br /> Methyl-tert-butyl Ether(MTBE) 22.8 1.0 ug/I 25.0 ND 91 55-145 <br /> Methyl-tert-butyl Ether(MTBE) 22.8 1.0 ug/1 25.0 ND 91 55-145 <br /> tert-Butanol(TBA) 136 10 ug/I 125 ND 109 65-140 <br /> Surrogate:4-Bromofluorobenzene 25.0 ug/1 25.0 100 80-120 <br /> Surrogate:4-Bromofluorobenzene 25.0 ug/1 25.0 100 80-120 <br /> Surrogate:Dibromofluoromethane 23.9 ug/I 25.0 95 80-120 <br /> Surrog&:Dibromofluoromethane 23.9 119/1 25.0 95 80-120 <br /> Surrogate:Toluene-d8 24.6 49/1 25.0 99 80-120 <br /> Surrogate: Toluene-d8 24.6 ug/l 25.0 99 80-120 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, <br /> except in full,without wriuen permission from TesiAmertca. 1U11062 <Page 39 of 67h <br />