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Client: Conestoga-Rovers&Assoc. (Emeryville)/SHELLAC Sample Results <br /> Project/Site: SAP 135703 TestAmerica Job ID: NVL1479 <br /> Method: SW846 8260B -Volatile Organic Compounds by EPA Method 82606 (Continued) <br /> Lab Sample ID: 11L2262-MSI <br /> Matrix: Water Client Sample ID: Matrix Spike <br /> Analysis Batch: U022174 Prep Type:Total <br /> Analyte <br /> Sample Sample Spike Matrix Spike Matrix Spike Prep Batch: 1IL2262_P I <br /> Result Qualifier %Rec. <br /> Ethyl tart-Butyl Ether A2500 Result qualifier Unit D %Rec Limits <br /> ND 2500 2780 <br /> Tart-Amyl Methyl Ether ND u9/L 111 60.138 <br /> 2500 2760 ug/L 110 61.138 <br /> Matrix Spike Matrix Spike I <br /> Surrogate %Recove <br /> ry Qualifier Limits <br /> 12-Dichloroelhaned4 109 <br /> 70-130 <br /> DibromoBuoromethane 99 <br /> Toluene-d898 <br /> 130 <br /> 95 70-130 <br /> 4-Bromolluorobenzene 105 <br /> 70.130 <br /> Lab Sample ID: 11 L2262-MSD1 <br /> Matrix: Water Client Sample ID: Matrix Spike Duplicate <br /> Analysis Batch: U022174 Prep Type:Total <br /> Sample Sample Spike Matrix Spike Dup Matrix Spike Dul Prep Batch: 1111-2262PAnalyte Result Qualifier %Rec. RPD <br /> Benzene Added Result Qualifier Unit D %Rec Limits <br /> 2630 2500 4950 _ RPD Limit <br /> Ethylbenzene ug/L <br /> 1630 93 75.133 Z 17 <br /> Toluene 1660 2500 3980 ug/L 94 79-139 2 <br /> 15 <br /> 2500 3970 <br /> Xylenes,total 8510 ug/L 92 75.136 2 75 <br /> ND <br /> Methyl tert-Butyl Ether 7500 14600 ug/L 81 74-141 0.6 15 Tertiary Butyl Alcohol 2500 2500Nou9/L 100 66.141 3 16 <br /> Diisopropyl Ether - -- 25000 15900 ug/L 64 50.183 q <br /> ND .. 2500. . -. 251 0 ... 32 <br /> Ethyl tart-Butyl Ether ND u9/L 100 54.147 --- 0.5 jg <br /> Tert-Amyl Methyl Ether2500 2830 ug/L 113 60-138 <br /> ND 2500 2 19 <br /> 2810 ug/L 112 61.138 2 15 <br /> Matrix Spike cup Matrix Spike Dup <br /> Surrogate %Recovery Qualifier L(m/ts <br /> 1,2-Dichlc,c thane-d4 109 <br /> --70--130 <br /> DibromoBuoromethane 98 <br /> 70-130 <br /> Toluene-d8 97 <br /> 70-130 <br /> 4-Bromopuorobenzene 104 <br /> 70.130 <br /> Lab Sample ID: 11L2636-BLK1 <br /> Matrix: Water Client Sample ID: Method Blank <br /> Analysis Batch: U022397 Prep Type:Total <br /> Blank Blank Prep Batch: 11L2635_P <br /> Analyte, Blank <br /> Qualifier <br /> Benzene ND RL MDL Unit D Prepared Analyzed DII Fac <br /> Ethylbenzene ND 0.500 u9/L 12/10/1111:37 12/20/1111:19 <br /> 0.500 1.00 <br /> Toluene ND u91L 12/10/1111:37 12/20/1111:19 1.00 <br /> Xylenes,total - -- -- -- - ND <br /> - -_ 0.500 _.._ _ ug/L 12/10/11 11:37 12/20/11 11:19 1.00 <br /> Methyl tart-Butyl Ether <br /> 0.500 ug/L 12/10/1111:37 12/20/1111:19 1.00 Tertiary Butyl Alcohol ND 0.500 ug/L 12/10/11 11:37 12/20/11 11:19 1.00 <br /> .. ._ ND <br /> Dilsopropyl Ether-- - -- - -- - - _10.0 ug/L 12/10/11 11:37 12/20/11 11:19 1.00g/L <br /> 0.500 u 12/10/11 11:37 1 2/20/11 11:19 1.00 <br /> Ethyl Cert-Butyl Ether ND <br /> Tert-Amyl Methyl Ether 0.500 ug/L 12/10/11 11:37 12/20/11 11:18 <br /> ND 0.500 1.00 <br /> ug/L 12/10/1111:37 12/20/1111:19 1.00 <br /> Blank Blank <br /> Surrogate %Recove <br /> ry Qualifier Limits <br /> 1,2-Dich/oroethane-dq 101 Prepared Analyzed DU Fac <br /> Dibromotluoromethane 70.130 12/10/11 11.37 t2_12011111.19 —100 <br /> 104 70_130 <br /> Toluene-d8 10012/10/11 11:37 12,20/1111:19 1,00 <br /> 70.130 12/10/11 11:37 12,20/11 11:19 1.00 <br /> Page 24 of 48 TestAmerica Nashville <br /> 12/22/2011 <br />