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QC Sample Results <br /> r <br /> Client: Conestoga-Rovers 8 Assoc. (Emeryville)I SHELL TestAmerica Job ID: NVL1479 <br /> Project/Site: SAP 135703 <br /> Method: SW846 8260B -Volatile Organic Compounds by EPA Method 82608 (Continued) <br /> Lab Sample ID:111.5135-BLK7 Client Sample ID: Method Blank <br /> Matrix: Water Prep Type:Total <br /> Analysis Batch: U022300 Prep Batch: 11L5135_P <br /> Blank Blank <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed oil Fac <br /> Toluene-d8 100 70.130 12119/i t 1240 _T21191112039 1.00 " <br /> 4-Bromofluorobenzene 98 70-130 12119/1112:40 12/19/1120:39 1.00 I <br /> Lab Sample ID: 11L5135-BSI Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type:Total <br /> Analysis Batch: U022300 Prep Batch: 11L5135_P <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Benzene 50.0 50.6 ug/L 101 80.121 <br /> Ethanol 5000 4950 ug/L 99 32.150 <br /> Ethylbenzene 50.0 51.7 ug/L 103 80-130 <br /> Toluene 50.0 51.1 ug/L 102 80.126 <br /> Xylenes,total 150 151 ug/L 100 80.132 <br /> Methyl tert-Butyl Ether 50.0 54.5 uglL 109 72-133 <br /> Tertiaary Butyl Alcohol 35-- 500 2 ug/L 70 54.150 <br /> Diisopropyl Ether 50.0 51.7 ug/L 103 62-137 <br /> Ethyl tert-Butyl Ether 50.0 53.9 ug/L 108 63-135 <br /> Tert-Amyl Methyl Ether 50.0 52.7 ug/L 105 63-135 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichloroethane-d4 111 70-130 <br /> Dibromofluoromethane 99 70.130 <br /> Toluene-d8 100 70-130 <br /> 4-Bromofluorobenzene 103 70_130 <br /> Lab Sample ID: 11 L5135-MS1 Client Sample ID: Matrix Spike <br /> Matrix:Water Prep Type:Total <br /> Analysis Batch: U022300 Prep Batch: 111-5136_P <br /> Sample Sample Spike Matrix Spike Matrix Spike %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Benzene 1260 500 1630 ug/L 75 75.133 <br /> Ethanol ND 50000 33700 ug/L 67 61-155 <br /> Ethylbenzene 401 500 870 ug/L 94 79.139 <br /> Toluene 684 500 1110110 <br /> ug/L 85 75.136 <br /> Xylenes,total 1250 1500 2530 ug/L 85 74.141 <br /> Methyl Cert-Butyl Ether ND 500 485 ug/L 97 66-141 <br /> Tertiary Butyl Alcohol ND 5000 2830 ug/L 57 50-183 <br /> Diisopropyl Ether ND 500 495 ug/L 99 54-147 <br /> Ethyl tert-Butyl Ether ND 500 522 ug/L 104 60.138 <br /> Tert-Amyl Methyl Ether ND 500 532 ug/L 106 61-138 <br /> Matrix Spike Matrix Spike <br /> Surrogate %Recovery Qualifier Limits <br /> 1,2-Dichloroethane-d4 112 70.130 <br /> Dibromofluoromethane 101 70.130 <br /> Toluene-d8 99 70.130 <br /> 4-Bromofluorobenzene 102 70-130 <br /> TestAmerica Nashville <br /> Page 29 of 48 112/22/2011 <br />