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TestAmerica <br /> T-iL LEADER IN ENVIRONMENTAL TESTING 17461 Derian Avenue.Suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Nary Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool . <br /> VOLATILE FUEL HYDROCARBONS BY GCIMS (CA LUFT) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-23(AS-13-15-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11D1513 10 130 99.6 4/13/2011 4/14/2011 <br /> Surrogate:Dibromofluoromelhane(55-140%) 90% <br /> Surrogate:Toluene-d8(60-140%) 95% <br /> Surrogate:4-Bromofluorobenzene(65-140916) 101 % <br /> Sample ID:IUD0863-25(AS-12-5-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-Cl2) TPH by GC/MS 1ID1531 0.20 1.5 1 4/13/2011 4/14/2011 <br /> Surrogate:Dibromofluoromethane(80-125%) 106% <br /> Surrogate: Toluene-d8(80-12001o) 106% <br /> Surrogate:4-Bromofluorobenzene(80-12001o) 99% <br /> Sample ID:IUD0863-26(AS-12-]0-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS I ID1513 10 180 100 4/13/2011 4/14/2011 <br /> Surrogate:Dibromofluoromethane(55-140916) 69% <br /> Surrogate:Toluene-d8(60-14091) 77% <br /> Surrogate:4-Bromofluorobenzene(65-14091) 87% <br /> Sample ID:IUD0863-28(AS-11-5-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11D1513 10 23 101 4/132011 4/14/2011 <br /> Surrogate:Dibromofluoromethane(55-140%) 100% <br /> Surrogate:Toluene-d8(60-140%) 102% <br /> Surrogate:4-Bromofluorobenzene(65-140%) 99% <br /> Sample ID:IUD0863-29(AS-I1-10-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11DI513 100 1600 1020 4/132011 4/152011 <br /> Surrogate:Dibromofluoromethane(55-140%) 96% Z3 <br /> Surrogate: Toluene-d8(60-140%) 99% Z3 <br /> Surrogate:4-Bromofluorobenzene(65-140%) 148% Z3 <br /> Sample ID:IUD0863-30(AS-11-15-Soil) Sampled:04/07/11 <br /> Reporting Units: mg/kg <br /> Volatile Fuel Hydrocarbons(C4-C12) TPH by GC/MS 11D1513 100 1100 996 4/13/2011 4/152011 <br /> Surrogate:Dibromofluoromethane(55-140%) 99% Z3 <br /> Surrogate:Toluene-d8(60-140%) 103% Z3 <br /> Surrogate:4-Bromofluorobenzene(65-1401o) 105% Z3 <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> Theresultspertain only to the samples testedln the laboratory. This reportshollnot be reproduced, ea <br /> exceptinfull,withouiwriiienpermissionfram TestAmerica. IUD0863 <pag7 .f3h <br />