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TestAmerica <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Dedan Avenne.Suite 100, 1,me,C.A 92614(949)261-1022 Fac:(949)260-3297 <br /> NEW <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 503013/826013) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-01(AS-22-5-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B IID1531 0.00099 0.0032 0.992 4/13/2011 4/13/2011 <br /> Ethylbenzene EPA 8260B 11D1531 0.00099 0.0016 0.992 4/13/2011 4/13/2011 <br /> Toluene EPA 82606 IID1531 0.00099 ND 0.992 4/13/2011 4/13/2011 <br /> Xylenes,Total EPA 82608 11D1531 0.0020 ND 0.992 4/13/2011 4/13/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11DI531 0.0020 ND 0.992 4/13/2011 4/13/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11DI531 0.0020 ND 0.992 4/13/2011 4/13/2011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260E I ID 1531 0.0020 ND 0.992 4/13/2011 4/13/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D1531 0.0020 ND 0.992 4/13/2011 4/13/2011 <br /> tett-Butanol(TBA) EPA 8260B I ID1531 0.020 ND 0.992 4/13/2011 4/13/2011 <br /> Surrogate:4-Bromofluorobensene(80-120%) 90% <br /> Surrogate:Dibromofluoromethane(80-12501o) 106% <br /> Surrogate: Toluene-0(80-120%) 106% <br /> Sample ID:IUD0863-05(AS-21-5-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D1513 0.050 0.97 101 4/13/2011 4/14/2011 <br /> Ethylbenzene EPA 82608 IIDI 513 0.050 2.7 101 4/13/2011 4/14/2011 <br /> Toluene EPA 8260B IID 1513 0.050 0.26 101 4/13/2011 4/14/2011 <br /> Xylenes,Total EPA 8260B IID1513 0.10 12 101 4/13/2011 4/14/2011 <br /> Di-isopropyl Ether(RIPE) EPA 8260E I ID1513 0.10 ND 101 4/13/2011 4/14/2011 R <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B I ID1513 0.10 ND 101 4/13/2011 4/14/2011 R <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11D1513 0.10 ND 101 4/13/2011 4/14/2011 R <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B I ID 1513 0.10 ND 101 4/13/2011 4/14/2011 R <br /> tert-Butanol(TBA) EPA 82608 I ID1513 1.0 ND 101 4/13/2011 4/14/2011 R-3,M2 <br /> Surrogate:4-Bromofluorobenzene(65-140%) 106% <br /> Surrogate:Dibromofluoromethane(55-14091o) 96% <br /> Surrogate:Toluene-&(60-140%) 97% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples rested in the laboratory. This report shall not be reproduced. <br /> exceptInfu/l,without writhmpermissionfrom TestAmerica, IUD0863 <Page9of37> <br />