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TestAmeric:a <br /> THE LEADER IN ENVIRONMENTAL TESTING 17461 Derien Avenue,Suite 100, Irvine,CA 92614(949)261-1022 Fax:(949)260-3297 <br /> �..�..a..va...r<r...emvwa..�.».a.:..w.e-..a.,.,�,az.��......,.e.���..,..�.,,... <br /> Conestoga-Rovers&Associates-Emeryville Shell Project ID: 3515 Navy Dr.,Stockton,CA <br /> 5900 Hollis St.,Suite A Sampled: 04/06/11-04/07/11 <br /> Emeryville,CA 94608 Report Number: IUD0863 Received: 04/08/11 <br /> Attention: Aubrey Cool <br /> VOLATILE ORGANICS by GC/MS(EPA 5030B/8260B) <br /> Reporting Sample Dilution Date Date Data <br /> Analyte Method Batch Limit Result Factor Extracted Analyzed Qualifiers <br /> Sample ID:IUD0863-09(AS-20-5-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B 11D1719 0.00099 ND 0.99 4/14/2011 4/14/2011 <br /> Ethylbenzene EPA 82608 11D1719 0.00099 ND 0.99 4/14/2011 4/14/2011 <br /> Toluene EPA 82608 IID 1719 0.00099 ND 0.99 4/14/2011 4/14/2011 <br /> Xylenes,Total EPA 8260B 11D1719 0.0020 ND 0.99 4/142011 4/14/2011 <br /> Di-isopropyl Ether(DIPE) EPA 8260B IID1719 0.0020 ND 0.99 4/14/2011 4/14/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 82608 11D1719 0.0020 ND 0.99 4/142011 4/142011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260E 1ID1719 0.0020 ND 0.99 4/142011 4/14/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B 11D1719 0.0020 ND 0.99 4/14/2011 4/14/2011 C <br /> tert-Butanol(TBA) EPA 8260B 11131719 0.020 ND 0.99 4/142011 4/14/2011 <br /> Surrogate:4-Bromofluarobenzene(80-120%) 97% <br /> Surrogate:Dibromofluoromethane(80-1250%) 110% <br /> Surrogate:Toluene-d8(80-120%) 105% <br /> Sample ID:IUD0863-10(AS-20-10-Soil) Sampled:04/06/11 <br /> Reporting Units: mg/kg <br /> Benzene EPA 8260B IIDI 531 0.0049 0.35 4.85 4/132011 4/14/2011 <br /> Ethylbenzene EPA 82608 11D1531 0.0049 0.37 4.85 4/132011 4/14/2011 <br /> Toluene EPA 8260B 11D1531 0.0049 ND 4.85 4/132011 4/142011 <br /> Xylenes,Total EPA 8260B 11D1531 0.0097 0.041 4.85 4/132011 4/142011 <br /> Di-isopropyl Ether(RIPE) EPA 8260B 11D1531 0.0097 ND 4.85 4/132011 4/14/2011 <br /> Ethyl tert-Butyl Ether(ETBE) EPA 8260B 11D1531 0.0097 ND 4.85 4/132011 4/142011 <br /> Methyl-tert-butyl Ether(MTBE) EPA 8260B 11D1531 0.0097 ND 4.85 4/132011 4/14/2011 <br /> tert-Amyl Methyl Ether(TAME) EPA 8260B I1D1531 0.0097 ND 4.85 4/132011 4/14/2011 <br /> tert-Butanol(TBA) EPA 8260B 11D1531 0.097 ND 4.85 4/132011 4/14/2011 <br /> Surrogate:4-Bromofluorobe=ene(80-120016) 107% <br /> Surrogate:Dibramofluoromethane(80-12501o) 106% <br /> Surrogate:Toluene-d8(80-120%) 106% <br /> TestAmerica Irvine <br /> Philip Sanelle <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory. This report shall not be reproduced <br /> except infull,without written permissionfrom Test4merica. IUDp863 <p¢g¢11 of3h <br />