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I 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:510-798-1620 Fax:510-798-1622 <br /> 24 http://Nvww.mccampbell.com E-mail:main@mccampbell.com <br /> J <br /> Advanced GeoEnvironmental <br /> Client Project ID: Steel Guard Date Sampled:08/18/97 <br /> Date Received:08/20/97 <br /> 1803 West March Lane,Ste A <br /> Stockton,CA 95207 Client Contact: Bill Little Date Extracted:08/20/97 <br /> Client P.O: Date Analyzed:08/20-08/22/97 <br /> Volatile Organics By GC/MS <br /> CPA method 8260 <br /> Lab ID 79957 <br /> Client ID P3-5 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone'' ND<200 trans-1,3-Dichloropropene ND<200 <br /> Benzene ND<200 Ethylene dibromide' ' ND<200 <br /> Bromobenzene ND<200 Ethylbenzene 2 0 <br /> Bromochloromethane ND<200 Hexachlorobutadiene ND<200 <br /> Bromodichloromethane ND<200 Iodomethane ND<200 <br /> Bromoform ND<200 Isopropylbenzene 110 <br /> Bromomethane ND<200 p-Isopropyl toluene 540 <br /> n-Butyl benzene 1400 Methyl butyl ketone"' ND<200 <br /> sec-Butyl benzene 360 1 Methylene Chloride" ND<200 <br /> tert-Butyl benzene 950 Methyl ethyl ketone"' ND<200 <br /> Carbon Disulfide D<200 Methyl isobutyl ketone' ' ND<200 <br /> Carbon Tetrachloride ND<200 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<200 Napthalene ND<200 <br /> Chloroethane ND<200 n-Propyl benzene 60. <br /> 2-Chloroethyl Vinyl Ether" ND<200 Styrene" ND<200 <br /> Chloroform ND<200 1,1,1,2-Tetrachloroeth3ne ND<200 <br /> Chloromethane ND< 1,1,2,2-Tetrachloroethane ND<200 <br /> 2-Chlorotoluene 090 Tetrachloroethene ND<200 <br /> 4-Chlorotoluene ND<200 Toluene""' ND<200 <br /> Dibrornochloromethane ND<200 1,2,3-Trichlorobenzene ND<200 <br /> 1,2-Dibromo-3-cltloropropane ND<200 1,2,4-Trichlorobenzene ND<200 <br /> Dibromomethane ND<200 1,1,1-Trichloroethane ND<200 <br /> 1,2-Dichlorobenzene ND<200 1,1,2-Trichloroethane ND<200 <br /> 1,3-Dichlorobenzene ND<200 Trichloroethene ND<200 <br /> 1,4-Dichlorobenzene ND<200 Trichlorofluoromethane ND<200 <br /> Dichlorodifluoromethane ND<200 1,2.3-Trichloropropane ND52,00 <br /> 1,1-Dichloroethane ND<200 1.2,4-Ti imethylbenzene 90 <br /> 1,2-Dichloroethane ND<200 1,3,5-Trimethylbenzene 1500 <br /> 1,1-Dichloroethene ND<200 Vinyl Acetate"" <200 <br /> cis-1,2-Dichloroethene N13<200 Vinyl Chloride'°' —ND <br /> trans-1,2-Dichloroethene ND<200 Xylenes,total '"' 500 <br /> 1,2-Dichloropropane ND<200 Comments: <br /> 1,3-Dichloropropane ND<200 Surrogate Recoveries('%,) <br /> 2,2-Dichloropropane ND<200 Dibromotluoromethane 101 <br /> 1,1-Dichloropropene ND<200 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND<200 4-Bromofluorobenzene 87 <br /> water and vapor samples are reported in uJL,soil and sludge samples in ug/kg,wipes in ughvipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone: (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than—5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)d ime thyl benzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />