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r <br /> MUM VERIFICATION IADORA'1.ORY IJLVSjg <br /> TANK 'TANK IPI I-O '1'l'f l-U 11-TX do L CI, Ile '1'CITAL METALS PC11 <br /> # CONTLIN'IS 8015 8015 8020 8010.. LEAD ICAP/ 8270 <br /> 826[1 82611 1120) 821 x420 AES or 81180 <br /> 7421 AA <br /> LEADED <br /> OAS X X x <br /> UNL OAS X x <br /> DIESEL x x <br /> KEROSUNH x x <br /> LINK MEL X X x x <br /> PROD. oil, x X <br /> CI Mort. <br /> SOLVENTS x x <br /> NONCI ILOR <br /> SOLVENTS X X X <br /> WASIn- <br /> USED Oil.. x x x X x x <br /> All analyses methods are designated EPA mellimis described In EPA SW 846, 'iiilyd RdIdon. 'These methods not found <br /> In SW 846, are specifically noted below. Refer to Ilia "SWRC11 LUFI'field Manual% Appendix A-20, Tablo 3-5 lot- <br /> detection ilnrits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 'Regional hoard Staff Recommendellons for <br /> Iullial Evaluation and hivestigatlon of US'I's' for the waste and motor oil detection 1111111s. <br /> Ilefetilon l.lr»lis that remain below fire MCL, STI.0 or Allowable LJutll of file corrtaminatrl In q+resdora will he accelFled, <br /> however laboralory shall Willie lire most conservative maleod. <br /> LABORATORY ANALYSES '13~RMINOCOOY: ' <br /> TPI1-0Total Petroleum Ilydrt"rbon, Gasoline, OC/f-1D (5030) 8015 mod or OC/MS 8260 <br /> 'IPI 1-1) Total Petroleum I Iydrmarbon, Dlcscl, CJC/FID (3550), 8015 rood or OC/MS 8260 i <br /> IVIA do I? 11enzene, 'Iirluenc, Xyierre & Etieyl I1enrene, OGPID 84120 or OCIMS 8260 <br /> CL Ile Chlortualed i lydrocarbon. OCIIISD 8010, OCjNiS 82411 <br /> TOTAL LEAD Talal lead, AA 7420, AA 7421 or [CP-AIC_S 6010 <br /> EDIT • Ethylene dibronrlde (DI IS-A11 1803), UC./MS 8240 (DI IS-LUFJ) <br /> OC-IIID Oas Chromalography, Flame lonizallon Delecllon <br /> ICAP or AA Inductively Coupled Plasma Atomic Eeutssion Speclronrelry 6010 or Atomic Absorpllon � <br /> SPeclromelry 7(XXI. Metalst Cad,nluny Chrnnriueu 111 arrd VI, Lead, 'Linc and Nickel. <br /> PCIS ' Polychlorinaled Iliphenyls, OC/MS 8270 or 808() <br /> Method 3050 Acid digestion <br /> Melhod 3540 Soahlel sample preparation <br /> Method 3550 Sonicallon sample prcparallon, extraction mclltod <br /> Method 5030 Purge and trap sample preparation. <br /> 4 QA/QC Quality Assurance/Quality (onlrol <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents ate to be used. I7,used capillary columns are <br /> Preferred to packed columns; a packed column may be used as a '[list cut' with "dirty samples or once lite hydrocarbons <br /> have been characterized and proper QA/AC Is followed. - <br />;i <br /> For Drltdcing water sources, IPPA recommends that lire 5(X1 series for volatile organics be used In preference to ilia 600 <br />�. aeries because the defection limits ora lower and the QA/QC Is better. Samples exhibiting any level of heavy mesal <br /> contalninatlon may require further analysis. PI IS-El ll) recommends holding lltese samples until disposal Is Indicated. <br /> i <br /> El 1 23 048 (Revised 7/1(1/92) Page 8 <br />