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Levine•Fri ckeliecon <br /> Section:Table C-5 <br /> Date Initiated: September 23, 1996 <br /> Revision No.: 6 <br /> Date Revised:October 16, 1998 <br /> Table C-5: Sample Handling Protocol for Organic Analysis Page 1 of 2 <br /> Lincoln Center, Stockton, California <br /> Test Method Sample Holding Times <br /> eter/Matrix Water/Soil Ref Sample Containers Mass/Volume Sample Preservative Water Soil/Vapor <br /> [EBTEX <br /> us Substances, 8010/8020 and 1 1-20 cc plastic or glass syringe 20 cc None N/A None - <br /> nd TPHg - Soil 8015 (modified) On-site <br /> (Mobile Lab) Mobile Lab <br /> TPHd and TPHo 8015 (modified) I 1 L amber bottle 1 L Cool 4°C 14 days N/A <br /> (Monitoring Wells) <br /> TPHg and We <br /> 8015/8020 2 3-40 mL glass vials; Teflon- 40 mL Acidify w/1:1 HCL to 14 days N/A <br /> (Phase I IRA GWETS (modified) backed septum; zero head space <pH 2; Cool 4°C <br /> Monitoring) <br /> Volatile Organic Compounds 8010 2 3-40 mL glass vials; Teflon- 40 mL Acidify w/1:1 HCL to 14 days N/A <br /> (PIPP Samples) backed septum; zero head space <pH 2; Cool 4°C <br /> Volatile Organic Compounds 8260A 2 3-40 mL glass vials; Teflon- 40 mL Acidify w/1:1 HCL to 14 days N/A <br /> Water (PIPP Samples and backed septum; zero head space <pH 2; Cool 4°C <br /> Phase I IRA GWETS <br /> Monitoring) <br /> Volatile Organic Compounds 8260A, 8260A 3 6-40 mL glass vials for Method 40 mL Acidify w/1:1 HCL to 14 days N/A <br /> Water (Monitoring Wells) (modified), and 8260A (modified) <pH 2; Cool 4°C <br /> 8015 (modified) 3-40 mL glass vials for Method <br /> 8015 and 8260A <br /> Volatile Organic Compounds 8260A 3 3-40 mL glass vials for Method 40 mL Acidify w/l:I HCL to 14 days N/A <br /> - Oxygenates - Water (Phase 8015 and 8260A <pH 2; Cool 40C <br /> I IRA GWETS Monitoring) <br /> Bioassy - Water (Phase I 1000, 1002, and 5 gallons 2.5 gallons Cool 4°C 36 hours N/A <br /> IRA GWETS Monitoring 1003 <br /> RIFS-QAPP-TBLC-5-REV6-04111:SRL Page 1 of 2 <br /> 10/15/98 <br />