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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> C Sample LR 111398-435049 <br /> Matnx WATER <br /> Prep Date 06/03/03 <br /> Analysis Date 06/03/03 <br /> ID#'s in Batch LR 111320, 111398, 111420, 111421, 111513, 111554 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Ree %Ree <br /> Test Method Result Added Spike Spk Dup MS MSD RPD <br /> TRPH 4181 ND 412 430 450 104 109 5 <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate %RPC LIMITS = 76 - 130 <br /> %REC-MS&MSD=Percent Recoier} of Matrix Spike&Matrix Spike Duplicate RPD LIMITS = 30 <br /> I <br /> PREPARATION BLANK 1 LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Rec L Limit H Limit <br /> ND 156 165 95 80% 120% <br /> Value=Preparation Blank Value ND=Not-Detected <br /> LCS Result=Lab Control Sample Result <br /> True=True Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> 611712003 4181_trph 0603w <br />