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' ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> 1 <br /> Sample 135691-551702 <br /> Matrix WATER <br /> Prep Date Sep 07-04 <br /> Analysis Date Sep 07-04 <br /> ID#'s in Batch LR 135691, 135841 <br />' MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units= mg/L <br /> 1 <br /> Sample Spike Matrix Matrix %Ree %Ree <br />' Test Method Result Added Spike Spk Dup MS MSD RPD <br /> TRPH 4181 ND 4 12 370 350 90 tis 6 <br /> 1 <br /> RPD=Relative Percent Diftei ence of Matrix Spike and Matt ix Spike Duplicate %REC LIMITS = 70 - 130 <br /> %REC-MS&MSD=Percent Recovery of Matrix Spike&Maty ix Spike Duplicate RPD LIMITS = 30 <br />' PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS � <br />' Value Result True %Rec L Limit H Limit <br /> ND 19 1650 - <br /> 115 80% 120% <br />' Value=Preparation Blank Value ND=Not-Detected <br /> LCS Result=Lab Control Sample Result <br />' Tine= True Value ojLCS L Limit III Limit=LCS Control Limits <br /> 1 <br /> 1 <br /> 1 <br />' 911412004 418 1 TRPH 0907 W <br />