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ASSOCIATED LABORATORIES <br /> QA REPORT FORM-METHOD 8260 1624/524.2 <br /> 11C Sample MS/MSD-Water Samples 134444-672 <br /> eppl <br /> sts Date Aug l7-04 <br /> es to LR 134331, 134428, 134281, I34335, 134444 <br /> (eporting Units= ug/L <br /> atrix Spike/Matrix Spike Dupbcate <br /> Spike Matrix Matrix %Rec %Rec QC Limits <br /> Cest:::=Result Added Spike Spk Dup MS MSD RPD RPD %REC <br /> 1,1-Diehloroethene ND 50 5103 5225 102 1052 22 59-172 <br /> TBE ND 50 4370 4451 87 89 2 24 62-137 <br /> Benzene ND 50 4496 44 19 90 88 2 24 62-137 <br /> nchloroethene ND 50 4423 4394 88 88 1 21 66-142 <br /> Toluene ND 50 4900 4787 98 96 2 21 59-139 <br /> hlorobenzene ND 50 46 94 47 43 94 95 1 21 60-133 <br /> QC Sample LCS/LCSD <br /> ralysis Date Aug 16-04 <br /> Lab Controlled Spike/Lab Controlled Spike Duplicate <br /> Sample Spike LCS LCS %Rec %Rec QC Limits <br /> Result Added Spike Spk Dup LCS <br /> LCS J) RPD RPD %REC <br /> 11-Dichloroethene ND 50 5230 53 94 105 108 3 22 59-172 <br /> TBE ND 50 4387 43 12 88 86 2 24 62-137 <br /> enzene ND 50 4477 44 86 90 90 0 24 62-137 <br /> nchloroethene ND 50 4630 4657 93 93 1 21 66-142 <br /> oluene ND 50 5071 50 13 101 100 1 21 59-139 <br /> hlamhenzene ND 50 48 96 48 62 98 97 1 21 b0-133 <br /> 140hod Blank=All ND <br /> SURROGATE { QC Limits : 70-135 ) <br /> Compounds DBFM 1,2-DCA Tol-d8 p-BFB <br /> MS 100 93 98 101 <br /> MSD 103 92 99 98 <br /> LCS 100 92 98 100 <br /> LCSD 101 92 97 102 <br /> BLANK# 1 103 106 103 99 <br /> BLANK#2 103 103 102 97 <br /> 9/1712004 8260 MSD-LCSD 0817 W <br />