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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> s <br /> QC Sample LR 122884-490885 <br /> Matrix WATER <br /> Prep Date 01/20/04 <br /> Analysts Date 01/20/04 <br /> M#'s in Batch LR 122881, 122882, 122883, 122884, 122943, 122984, 122990, 122991, 122992, 122993, <br /> LR 123006 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Rec %Rec <br /> Test Method Result Added Spike Spic Dup MS MSD RPD <br /> TRPH 418 i ND 41 3 80 4 40 92 107 15 <br /> D=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate %REC LIMITS = 70 - 130 <br /> *EC-MS&MSD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate RPD LIMITS = 30 <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Ree L.Limit H.Lunit <br /> ND 15 8 165 96 80% 1 120% <br /> Value=Preparation Blank Value ND=Not-Detected <br /> LCS Result=Lab Control Sample Result <br /> True=Tnie Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> 0 <br /> 1/2612004 418 1_trpJi_0120w <br />