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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> QC Sample LR 67851 -285 <br /> Matrix WATER <br /> Prep Date 02/22/01 <br /> Analysis Date 02/22/01-02123101 <br /> ID#'s to Batch LR 67851,68007,68011 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units=ug/L <br /> Sample Spike Matrix Matrix %Rec %Ree <br /> Test Method Result Added Spike [Spike Du MS MSD RPD <br /> TPH J 8015M-G ND 520 461 472 887 908 2 4 <br /> SVD=Not Detected <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate %REC LIMITS = 70 - 130 <br /> %REC-MS&MSD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate i fp LIMITS 30 <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Value Result True %Rec L Limit H Limit <br /> ND 480 520 42 3 80% 120% <br /> LCS Result=Lab Control Sample Result ` <br /> True=True Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> • <br /> 03/05/2001 8015g_tph_0222,A xls <br />