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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> AidO HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample 1D: B1@7.5-8' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-02— <br /> Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit Dil.Factor QUAL Date Analyzed Anaiyst Seq.# <br /> DIESEL RANGE ORGANICS MCL CA DRO Units:mg/Kg <br /> Diesel Range Organics 82 10 5 07/02/04 6:09 AE 2305398 <br /> Surr.n-Pentacosane 99.8 % 20-154 5 07/02/04 6:09 AE 2305398 <br /> Pre Method 1Preo Date 1Prey Initials lPrepFactor <br /> SW35508 06129!200413:47 DMN 1.00 <br /> Qualifiers: ND/.0-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated,Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> `-Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 4 <br /> 71M 3:0&12 PM <br />