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� ! s <br /> HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> HOUSTON,7x-77054 <br /> (713)660-0901 <br /> Client Sample ID: B2@4.0-4.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-05 <br /> Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit Dil.Factor QUAL Date Analyzed Analyst Seq.# <br /> DIESEL RANGE ORGANICS <br /> MCL CA DRO Units: mglKg <br /> Diesel Range Organics 82 10 5 _ 07/02/04 6:48 AE <br /> Surr:n-Pentacosane 2305399 <br /> 68.6 °� 20-154 5 07/02/04 6:48 A E 2305399 <br /> Pre Method Pre Date Pre fnitfals Pre Factor <br /> SW35508 06129/200413:47 PMN Prs <br /> DIESEL RANGE ORGANICS-TCLP MCL CA DRO Units. mglL <br /> Diesel Range Organics 3 0.5 1 <br /> 07/03/04 21:34 AE 2299B71 <br /> Surr:n-Pentacosane 90.4 % 20-150 1 07/03/04 29:34 AE <br /> 2299671 <br /> Pre Method Prep Date - Pre Initials. Pre Factor Leach Method Leachate Date Leach Initials <br /> SW3510C 06128/200410:33 K_L 1A0SW1319M D6/251200415:39 E 5 <br /> MERCURY,TOTAL MCL SW7471A Units:mg/Kg Mercury 0.0426 0.03 <br /> 1 0710310414:34 JAB 2298912 <br /> Prep Method- <br /> Pre Date Pre Initials Pre Factor <br /> SW7471A 07/02/2004 9:50 JAS 1.00 <br /> METALS BY METHOD 60106,TOTAL MCL SW6010B Units: mg/Kg <br /> Antimony 6.46 0.5 1 07!0310417:07 NS 2299067 <br /> 3 <br /> Arsenic .92 0.5 1 0710310417:07 NS 2299067 <br /> Lead 6.84 0.5 1. 07/03/04 17:07 NS 2299067 <br /> Selenium 0.712 0.5 1 0710310417:07 NS 2299067 <br /> Thallium 3.27 0.5 1 0710310417:07 NS 2299067 <br /> Barium 85.5 0.5 1 07/02/04 22:31 WV <br /> Beryllium 2298551 <br /> ND 0.5 1 07/02/04 22:31 MW 2298551 <br /> Cadmium ND 0.5 1 07/03/04 21:51 MW 2300345 <br /> Chromium 22.1 1 1 07/02/04 22.31 MW 2298551 <br /> Cobalt 10.9 1 1 07/02/04 22:31 MW 2298551 <br /> Copper 22.1 1 1 07/02/04 22:31 MW 2298551 <br /> Molybdenum ND 2 1 07/02/04 22:31 MW 2298551 <br /> Nickel 34.4 2 1 07/02/04 22:31 MW 2298551 <br /> Silver ND 1 1 07/02/04 22:31 MW 2298551 <br /> Vanadium 41.2 0.5 1 07/02/04 22:31 IVW 2298551 <br /> Zinc 43.6 2 1 07/02/04 22:31 NW 2298551 <br /> Oren Method jPreo Date PreD Initials 1PreD Factor <br /> SW3050B 07/02/2004 7:01 SE 1.00 <br /> Qualifiers: NDIU-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> 8-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> '-Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 7 <br /> 71VO4 3:06:15 PM <br />