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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> e HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B2@4.0-4.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-05 <br /> Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit Oil. Factor QUAL Date Analyzed Analyst Seq.# <br /> Bis(2-ethyl hexyl)phtha late NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Butyl benzyl phthalate NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Carbazole NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Chrysene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Di-n-butyl phthalate ND 1600 5 07/04/04 2:13 GO 2301997 <br /> Di-n-octyl phthalate NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Dibenz(a,h)anthracene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Dibenzofuran NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Diethyl phthalate NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Dimethyl phthalate NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Fluoranthene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Fluorene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Hexachlorobenzene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Hexachlorobutadiene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Hexachiorocyclopentadiene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Hexachloroethane ND 1600 5 07/04/04 2:13 GQ 2301997 <br /> Indeno(1,2,3-cd)pyrene NO 1600 5 07104/042:13 GO 2309997 <br /> Isophorone NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> N-Nitrosodi-n-propylamine NO 1600 5 07/04/04 2.13 GQ 2301997 <br /> N-Nitrosodiphenylamine NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Naphthalene ND 1600 5 07/04/04 2:13 GQ 2301997 <br /> Nitrobenzene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Pentachlorophenol NO 4000 5 07/04/04 2:13 GQ 2301997 <br /> Phenanthrene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Phenol ND 1600 5 07/04/04 2:13 GQ 2301997 <br /> Pyrene NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Pyridine NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> 2-Methylphenol NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> 3&4-Methylphenol NO 1600 5 07/04/04 2:13 GQ 2301997 <br /> Surr:2,4,6-Tribromophenol 68.0 % 19-135 5 07/04/04 2:13 GQ 2301997 <br /> Surr:2-Fiuorobiphenyl 44.1 % 15-140 5 07/04/04 2:13 GQ 2301997 <br /> Surr:2-Fluorophenol 48.0 % 15-122 5 07/04/04 2:13 GO 2301997 <br /> Surr:Nitrobenzene-d5 45.3 % 10-134 5 07/04/04 2:13 GQ 2309997 <br /> Sum.Phenol7d5. 48.0 % 10-123 5 07/04/04 2:13 GQ 2301997 <br /> Surr:Terphenyl-d14 47.1 % 18-166 5 07/04/04 2:13 GQ 2301997 <br /> 1Preo Method 1prep Oate jPreo Initials Pre Factor <br /> SW3550B 106i2912OD411.24 JDMN 11.00 <br /> Qualifiers: NDIU-Not Detected at the Reporting Limit nMCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> '-Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 9 <br /> 7S%396:16 PM <br />