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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B2@4.0-4.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-05 <br /> Site: Shell-Tracy Pump Station <br /> AnalyseslMethod Result Rep.Limlt Dil.Factor QUAL Date Analyzed Analyst Seq.# <br /> VOLATILE ORGANICS BY METHOD 82608 MCL SW8260B Units:ug/Kg <br /> 1,1,1,2-Tetrachioroethane NO 5 1 06127/04 22:15 ME 2288563 <br /> 1,1,1-Trichloroethane ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,1,2,2-Tetrachloroethane NO 5 1 06127/04 22:15 NE 2288563 <br /> 1,1,2-Trichloroethane NO 5 1 06/27/04 22:15 ME 2288563 <br /> 1,1-Dichlorosthane ND 5 1 06/27/04 22:15 NE 2288563 <br /> ' 1,1-Dichloroethene ND 5 1 06127/04 22:15 ME 2288563 <br /> 1,1-Dichloropropene ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2,3-Trichlorobenzene ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2,3-Trichloropropane NO 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2,4-Trichlorobenzene ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2,4-Trimethylbenzene NO 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2-Dibromo-3-chloropropane ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2-Dibromoethane ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,2-Dichlorobenzene NO 5 1 06/27/04 22:15 NE 2288563 <br /> 1,2-Dichloroethane ND 5 1 06127/04 22:15 NE 2288563 <br /> 1,2-Dichloropropane ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,3,5-Trimethylbenzene ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,3-Dichiorobenzene ND 5 1 06/27/04 22:15 ME 2288563 <br /> 1,3-Dichloropropane NO 5 1 06/27/04 22:15 ME 2288563 <br /> 1,4-Dichlorobenzene ND 5 1 06/27/04 22:15 NE 2288563 <br /> 2,2-Dichloropropane ND 5 1 06/27/04 22:15 ME 2288563 <br /> 2-Butanone ND 20 1 06/27/04 22:15 ME 2288563 <br /> 2-Chloroethyl vinyl ether ND 10 1 06/27/04 22:15 ME 2288563 <br /> 2-Chlorotoluene NO 5 1 06/27/04 22:15 ME 2288563 <br /> 2-Hexanone NO 10 1 06/27/04 22:15 NE 2288563 <br /> 4-Chlorotoluene NO 5 1 06/27/04 22:15 ME 2288563 <br /> 4-Isopropyltoluene ND 5 1 06/27/04 22:15 ME 2288563 <br /> 4-Methyl-2-pentanone ND 10 1 06/27/04 22:15 ME 2288563 <br /> Acetone 150 100 1 06/27/04 22:15 ME 2288563 <br /> Acrylonitrile ND 50 1 06/27/04 22:15 ME 2288563 <br /> Benzene NO 5 1 66/27/04 22:15 NE 2288563 <br /> Bromobenzene ND 5 1 06/27/04 22:15 ME 2288563 <br /> Bromochloromethane NO 5 1 06/27/04 22:15 ME 2288563 <br /> Bromodichloromethane ND 5 1 06/27/04 22:15 NE 2288563 <br /> Bromoform ND 5 1 06/27/04 22:15 ME 2288563 <br /> Bromomethane ND 10 1 06/27/04 22:15 ME 2288563 <br /> Carbon disuiFide NO 5 1 06/27/04 22:15 ME 2288563 <br /> Carbon tetrachloride NO 5 1 06/27/04 22:15 ME .2288563 <br /> Chiorobenzene NO 5 1 06/27/04 22:15 ME 2288563 <br /> Chloroethane NO 10 1 06/27/04 22:15 ME 2288563 <br /> Qualifiers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the assodated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> '-Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 11 <br /> 719814 306:17 PM <br />