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HOUSTON LABORATORY <br /> za�"���'WAE— 8880 INTERCHANGE DRIVE <br /> HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B2@11.5-12' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-07 <br /> Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit Dil.Factor QUAL Date Analyzed Analyst Seq.# <br /> DIESEL RANGE ORGANICS MCL CA DRO Units:mg/Kg <br /> Diesel Range Organics 14 2 1 07/01/04 22:17 AE 2305388 <br /> Surr:n-Pentacosane 93.2 % 20-154 1 07/01/04 22:17 AE 2305388 <br /> jPreo Method Orep Date IPMV Inipals Pre Factor <br /> SW35506 106129Y200413:47 JDMN 11.00 <br /> MERCURY,TOTAL MCL SW7471A Units:m <br /> Mercury ND 0.03 1 0710310415:02 JAB 2298923 <br /> 1Prep Method 1PreD Date I Pre Inifials Orep f=actor <br /> SW7471A 07102/20049:50 IJAB 1.00 <br /> METALS BY METHOD 60108,TOTAL. MCL SW6010B Units:mglKg <br /> Antimony 6.67 0.5 1 0710310417:13 NS 2299068 <br /> Arsenic 4.59 0.5 1 0710310417:13 NS 2299068 <br /> Lead 5.72 0.5 1 0710310417:13 NS 2299068 <br /> Selenium ND 0.5 1 0710310417:13 NS 2299068 <br /> Thallium ND 0.5 1 0710310417:13 NS 2299068 <br /> Barium 189 0.5 1 07/02/04 22:35 MW 2298552 <br /> Beryllium ND 0.5 1 07/02/04 22:35 MW 2298552 <br /> Cadmium ND 0.5 1 07/03/04 21.55 MW 2300346 <br /> Chromium 35.8 1 1 07/02/04 22:35 MW 2298552 <br /> Cobalt 9.25 1 1 0502/04 22:35 MW 2298552 <br /> Copper 12.9 1 1 07/02/04 22:35 MW 2298552 <br /> Molybdenum ND 2 1 07/02/04 22:35 MW 2298552 <br /> Nickel 47.4 2 1 07/02/04 22:35 MW 2298552 <br /> Silver ND 1 1 07/02/04 22:35 MW 2298552 <br /> Vanadium 37.3 0.5 1 07/02/04 22:35 MW 2298552 <br /> Zinc 40 2 1 07/02/04 22:35 MW 2298552 <br /> Freo Method JPrep Date Orep initials 1PreQ Factor <br /> SW30506 07/02/2004 7:01 ISE 11.00 <br /> I� <br /> Qualifiers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> -Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 14 <br /> 71WN 3,0620 PM <br />