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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> ® HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample 11): B2@11•.5-12' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-07- <br /> Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit DII.Factor QUAL Date Analyzed Analyst Seq.# <br /> Bis(2-ethyihexyl)phthalate ND 330 1 071041041:07 GQ 2301995 <br /> Butyl benryf phthalate ND 330 1 07/04/04 1:07 GQ 2301995 <br /> Carbazole NO 330 1 071041041:07 GO 2301995 <br /> Chrysene NO 330 1 071041041:07 GQ 2301995 <br /> Di-n-butyl phthalate NO 330 1 07/04/04 1:07 GQ 2301995 <br /> Di-n-octyl phthalate NO 330 1 07/04/04 1:07 GQ 2301995 <br /> Dibenz(a,h)anthracene NO 330 1 071041041:07 GQ 2301995 <br /> Dibenzofuran NO 330 1 07/041041:07 GQ 2301995 <br /> Diethyl phthalate NO 330 1 07/04/04 1:07 GQ 2301995 <br /> Dimethyl phthalate NO 330 1 07/04/04 1:07 GQ 2301995 <br /> Fiuoranthene NO 330 1 071041041:07 GQ 2301995 <br /> Fluorene ND 330 1 071041041:07 GQ 2301995 <br /> Hexachlorobenzene NO 330 1 071041041:07 GQ 2301995 <br /> Hexachlorobutadiene NO 330 1 07104/041:07 GQ 2301995 <br /> Hexachlorocyclopentadiene NO 330 1 071041041:07 GQ 2301995 <br /> Hexachloroethane NO 330 1 071041041:07 GQ 2301995 <br /> Indeno(1,2,3-cd)pyrene ND 330 1 07/04/04 1:07 GQ 2301995 <br /> �. Isophorone NO 330 1 07/041041:07 GQ 2301995 <br /> N-Nitrosodi-n-propylamine NO 330 1 071041041:07 GQ 2301995 <br /> N-Nitrosodiphenylamine NO 330 1 071041041:07 GQ 2301995 <br /> Naphthalene NO 330 1 071041041:07 GQ 2301995 <br /> Nitrobenzene ND 330 1 071041041:07 GQ 2301995 <br /> Pentachlorophenol NO 800 1 071041041:07 GQ 2301995 <br /> Phenanthrene NO 330 1 071041041:07 GQ 2301995 <br /> Phenol ND 330 1 071041041:07 GQ 2301995 <br /> Pyrene NO 330 1 071041041:07 GQ 2301995 <br /> Pyridine NO 330 1 071041041:07 GO 2301995 <br /> 2-Methylphenol NO 330 1 071041041:07 GQ 2301995 <br /> 3&4-Methyiphenol NO 330 1 071041041:07 GQ . 2301995 <br /> Surr:2,4,6-Tdbromophenol 68.1 % 19-135 1 071041041:07 GQ 2301995 <br /> Sum 2-Fluorobiphenyl 44.2 % 15-140 1 07/04/04 1:07 GQ 2301995 <br /> 5urr.2-Fluorophenol 40.1 % 15-122 1 071041041:07 GQ 2301995 <br /> Surr.Nitrobenzene-d5 40.1 % 10-134 1 07/04/04 1:07 GQ 2301995 <br /> Surr:Phenol-d5 44.1 % 10-123 1 07/04104 1:07 GQ 2301995 <br /> Sum.Terphenyl-d14 58.9 % 18-166 1 07/04/04 1:07 GQ 2301995- <br /> IlDreD Method lPrep Date Oren Initials Pre Factor <br /> SW35506 1061291200411:24 JDMN J1.00 <br /> Qualifiers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> -Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 16 <br /> 719IU 3:0621 PM <br />