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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> C HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: B2@11.5-12' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-07 <br /> Site: Shell-Tracy Frump Station <br /> Analyses/Method Result Rep.Limit Dil.Factor QUAL Date Analyzed Analyst Seq.# <br /> Chloroform ND 5 1 06/27/04 22:42 ME 2288564 <br /> Chloromethane ND 10 1 06/27/04 22:42 ME 2288564 <br /> dibromochforomethane NO 5 1 06/27/04 22:42 ME 2288564 <br /> Dibromomethane ND 5 1 06/27/04 22:42 ME 2288564 <br /> Dichlorodifluoromethane ND 10 1 06/27/04 22:42 ME 2288564 <br /> Ethyibenzene ND 5 1 06/27/04 22.42 ME 2288564 <br /> Hexachlorobutadiene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Isopropylbenzene ND 5 1 06127104.22:42 ME 2288564 <br /> Methyl tert-butyl ether ND 5 1 06/27/04 22:42 ME 2288564 <br /> Methylene chloride ND 5 1 06127/04 22:42 ME 2288564 <br /> n-Butylbenzene ND 5 1 06127!04 22:42 ME 2288564 <br /> n-Propylbenzene ND 5 1 06/27/04 22.42 ME 2288564 <br /> Naphthalene ND 5 1 06/27/04 22:42 WE 2288564 <br /> sec-Butylbenzene NO 5 1 06/27/04 22:42 ME 2288564 <br /> Styrene ND 5 1 06/27/04 22:42 ME 2288564 <br /> tert-Butylbenzene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Tetrachloroethene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Toluene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Trichloroethene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Trichlorofluoromethane ND 5 1 06/27/04 22:42 ME 2288564 <br /> Vinyl acetate ND 10 1 06/27/04 22:42 ME 2288564 <br /> Vinyl chloride ND 10 1 06/27/04 22:42 ME 2288564 <br /> cis-1,2-Dichloroethene ND 5 1 06/27/04 22:42 ME 2288564 <br /> cis-1,3-Dichloropropene ND 5 1 06/27/04 22:42 ME 2288564 <br /> m,p-Xylene ND 5 1 06/27/04 22:42 ME 2288564 <br /> o-Xylene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Ira ns-l,2-Dichloroethene NO 5 1 06/27/04 22:42 ME 2288564 <br /> trans-1,3-Dichloropropene ND 5 1 06/27/04 22:42 ME 2288564 <br /> Xylenes,Total NO 5 1 06/27/04 22:42 ME 2288564 <br /> 72-Dichloroethene(total) ND 5 1 06/27/04 22:42 ME 2288564 <br /> Surr: 1,2-Dichloroethane-d4 96.0 No 64-130 1 06/27/04 22:42 ME 2288564 <br /> Surr:4-Bromofluorobenzene 100 % 62-130 1 06/27/04 22:42 ME 2288564 <br /> Surr.Toluene-d8 88.0 % 70-140 1 06/27/04 22:42 ME 2288564 <br /> i <br /> 1 <br /> Quallflers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> '-Surrogate Recovery Outside Advisable QC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and PQL 04061001 Page 18 <br /> 71BO4 3:0623 PM <br />