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HOUSTON LABORATORY <br /> ' 8880 INTERCHANGE DRIVE <br /> ® HOUSTON,TX 77054 <br /> (713)660-0901 <br /> Client Sample ID: 87@2.0-2.5' Collected: 06/21/2004 0:00 SPL Sample ID: 04061001-14 <br /> ' Site: Shell-Tracy Pump Station <br /> Analyses/Method Result Rep.Limit DII.Factor QUAL Date Analyzed Analyst Seq.# <br /> DIESEL RANGE ORGANICS MCL CA DRO Units: mg/Kg <br /> Diesel Range Organics 8.8 2 1 07/02/04 3:32 AE 2305394 <br /> Surr:n-Pentacosane 90.8 % 20-154 1 07/02/04 3:32 AE 2305394 <br /> 1PreQ Method PreD Date IlPrep Initials Pre Factor <br /> SW3550B 1061291200413:47 JDMN 11.0o <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> Qualifiers: ND/U-Not Detected at the Reporting Limit >MCL-Result Over Maximum Contamination Limit(MCL) <br /> B-Analyte detected in the associated Method Blank D-Surrogate Recovery Unreportable due to Dilution <br /> .-Surrogate Recovery Outside Advisable OC Limits MI-Matrix Interference <br /> J-Estimated Value between MDL and POL 04061001 Page 29 <br /> M04 3:05:30 PM <br />