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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> I ® HOUSTON,TX 77054 <br /> Quality Control Report (713)660-0901 <br /> Shell Oil Company <br /> INC#NIA <br /> Analysis: Semivolatile Organics by Method 8270C WorkOrder: 040610DI <br /> Method: SW8270C Lab Batch ID: 39054 <br /> Method Blank Samples in Analytical Batch: <br /> RunID: P_040701A-2296859 Units: ug/kg <br /> Lab Samg'le ID Client Sample ID <br /> Analysis Date: 07/01/2004 19:04 Analyst: GO 04061001-05A 82@4.0-4.5' <br /> 'reparation Date: 06/29/2004 11:24 Prep By: DMN Method SW3550B 04061001-07A B2@11.5-12' <br /> 04061001-10A B5@2.0-2.5' <br /> Analyte Result Rep Limit <br /> 12 4-Trichiorobenzene NO 330 <br /> 12-Dichlorobenzene ND 330 <br /> 12-Di hen Ih drazine ND 330 <br /> 13-Dichlorobenzene ND 330 <br /> 14-Dichlorobenzene NO 330 <br /> 2 4 5-Trichloro henol <br /> NO 800 <br /> 2,4,6-Trichlorophenol ND 330 <br /> 2 4-Dichloro henol ND 330 <br /> 2,4-Dimethylphenol ND 330 <br /> 2 4-Dinitrohenol Np 800 <br /> 2 4-Dinitrotoluene NO 330 <br /> 2,6-Dinitrotoluene NO 330 <br /> 2-Chbmna hthalene NO 330 <br /> 2-Chloro henol NO 330 <br /> 2-Meth Ina hthalene NO 330 <br /> 2-Nitroaniiine NO 800 <br /> 2-Nitro henol ND <br /> 3-Nit 330 <br /> 3 Nit ichlor.benzidine NO 330 <br /> aniline ND 800 <br /> 4 6-Dinitro-2-meth I henol NO 800 <br /> 4-13romo hen hen ether ND 330 <br /> 4-Chloro-3-meth I henol NO 330 <br /> 4-Chloroaniline NO 330 <br /> 4-Chlorohen I phenvi ether NO 330 <br /> 4-Nitroaniline NO $00 <br /> 4-Nitro henol ND $00 <br /> Acenaphthene NO 330 <br /> Acena hth leve NO 330 <br /> Aniline NO 330 <br /> Anthracene NO 330 <br /> Benz(a)anthracene NO 330 <br /> Benzo(a)pyrene NO 330 <br /> Benzo b fluoranthene NO 330 <br /> Benzo h i lens NO 330 <br /> Benzo k uoranthene NO 330 <br /> Benzoic acid NO 1600 <br /> SeWA alcohol ND 330 <br /> Bis 2-chloroetho methane NO 330 <br /> Bis2-chlaroeth I ether NO 330 <br /> Bis 2-chloroiso rother NO 330 <br /> Bis(2-eth he hthalate NO 330 <br /> HuW benzyl Phthalate NO 330 <br /> Carbazole NO 330 <br /> Ch ere NO 330 <br /> Di-n-butyi hthalate NO 336 <br /> Dk-oct)4 phthalate NO 330 <br /> Dibenz a h anthracene NO 330 <br /> Dibertzofuran ND 330 <br /> Qualifiers: NDN-Not Detected at the Reporting Limit MI-Matrix interference <br /> B-Analyte detected in the associated Method Blank D-Recovery Unreportable due to.Dilution <br /> J-Estimated value between MDL and PQL `-Recovery Outside Advisable QC Limits <br /> NIC-Not Calculated-Sample concentration is greater than 4 times the amount of spike added.Control limits do not apply. <br /> The percent recoveries for QC samples are correct as reported.Due to significant figures and 04061001 Page 43 <br /> rounding,the reported RPD may differ from the displayed RPD values but is correct as reported. <br /> 719!04 3:06:58 FM <br />