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HOUSTON LABORATORY <br /> 8880 INTERCHANGE DRIVE <br /> HOUSTON,TX 77054 <br /> Quality Control Report (713)660-0901 <br /> Shell Oil Company <br /> INC#N1A <br /> Analysis: Volatile Organics by Method 8260B WorkOrder: 04061001 <br /> Method: SW8260B Lab Batch ID: R114853 <br /> Method Blank Samples in Analytical Batch:_ <br /> Run1D: M_040627A-22aa546 Units: ug/Kg <br /> Lab Sample ID Client Sam le ID <br /> Analysis Date: 06/27/2004 14:12 Analyst: ME 04061001-05A 82@4.04,5' <br /> 04061001-07A B2@11.5-12' <br /> 04061001-10A 85@2.0-2.5' <br /> Analyte Result Rep Limit <br /> 1112-Tetrachloroethane ND 5.0 <br /> 111-Trichloroethane ND 5.0 <br /> 1 1.2 2-Tetrachloroethane ND 5A <br /> 112-Trichloroethane ND 5.0 <br /> 11-Dichloroethane <br /> NO 5.0 <br /> 11-Dichloroethene ND 5.0 <br /> 1 1-Dichloro ro ene ND 5.0 <br /> 12 3-Trirhlorobenzene ND 5.0 <br /> 1 2 3-Trichloro ro ne ND 5.0 <br /> 1 2 4-Trichlorobenzene ND 5.0 <br /> 12 4-Trimeth (benzene ND 5.0 <br /> 1 2-Dibromo-3-chlor-------- ND 5.0 <br /> 1,2-Dibromoethane ND 5.0 <br /> 12-Dichlorobenzene ND 5.D <br /> 12-Dichloroethane ND 5.0 <br /> 1 2-Dichlororone ND 5.0 <br /> 1 3 5-Trimeth (benzene NO 5.0 <br /> 13-Dichlorobenzene ND 5"0 <br /> 1 3-Dichlororoane ND 5.0 <br /> 14-Dichlorobenzene ND 5.0 <br /> 2 2-Dichlore ro ane ND 5.0 <br /> 2-8utanone ND 20 <br /> 2-Chloroeth I vin I ether ND 10 <br /> 2-Chlorotoluene ND 5.0 ' <br /> 2-Hexanone NO 10 <br /> 4-Chlorotoluene ND 5.0 <br /> 4-Iso ro (toluene ND 5.0 <br /> 4-Meth 1-2- Marion ND 10 <br /> Acetone ND 100 <br /> A lonMle ND 50 <br /> Benzene ND 5.0 <br /> Bromobenzene ND 5.0 <br /> Bromochloromethane ND5.0 <br /> Bromodichioromethane ND 5.0 <br /> ' Bromoform ND 5.0 <br /> Sromomethane ND 10 <br /> Carbon disulfide ND 5.0 <br /> Carbon tetrachloride ND 5.0 <br /> Chlorobenzene ND 5.0 <br /> Chloroethane ND 10 <br /> Chloroform NO 5.0 <br /> Chloromethane ND 10 <br /> Dibromochloromethane ND 5.0 <br /> ' Dibmmomethane ND 5.0 <br /> Dichiorodifluoromethane ND 10 <br /> Eth benzene ND 5.D <br /> Hexachlorobutadiene ND 5.0 <br /> 1-soproo0benzene ND 50 <br /> Qualifiers: NDN-Not Detected at the Reporting Limit MI-Matrix Interference <br /> B-Analyte detected in the associated Method Blank D-Recovery Unreportable due to Dilution <br /> J-Estimated value between MDL and PQL *-Recovery Outside Advisable QC Limits <br /> NIC-Not Calculated-Sample concentration is greater than 4 times the amount of spike added.Control limits do not apply. <br /> The percent recoveries for QC samples are correct as reported.Due to significant figures and 04061001 Page 50 <br /> rounding,the reported RPD may differ from the displayed RPD values but is correct as reported. <br /> 719104 3:07:03 Pial <br />